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Reflux Still
Reflux is a technique involving the condensation of vapors and the return of this condensate to the system from which it originated. It is used in industrial and laboratory distillations. It is also used in chemistry to supply energy to reactions over a long period of time. Reflux in industrial distillation The term ''reflux'' is very widely used in industries that utilize large-scale distillation columns and fractionators such as petroleum refineries, petrochemical and chemical plants, and natural gas processing plants. In that context, reflux refers to the portion of the overhead liquid product from a distillation column or fractionator that is returned to the upper part of the column as shown in the schematic diagram of a typical industrial distillation column. Inside the column, the downflowing reflux liquid provides cooling and condensation of the upflowing vapors thereby increasing the efficiency of the distillation column. The more reflux provided for a given num ...
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Continuous Binary Fractional Distillation
Continuity or continuous may refer to: Mathematics * Continuity (mathematics), the opposing concept to discreteness; common examples include ** Continuous probability distribution or random variable in probability and statistics ** Continuous game, a generalization of games used in game theory ** Law of Continuity, a heuristic principle of Gottfried Leibniz * Continuous function, in particular: ** Continuity (topology), a generalization to functions between topological spaces ** Scott continuity, for functions between posets ** Continuity (set theory), for functions between ordinals ** Continuity (category theory), for functors ** Graph continuity, for payoff functions in game theory * Continuity theorem may refer to one of two results: ** Lévy's continuity theorem, on random variables ** Kolmogorov continuity theorem, on stochastic processes * In geometry: ** Parametric continuity, for parametrised curves ** Geometric continuity, a concept primarily applied to the conic s ...
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Chemical Reaction
A chemical reaction is a process that leads to the IUPAC nomenclature for organic transformations, chemical transformation of one set of chemical substances to another. Classically, chemical reactions encompass changes that only involve the positions of electrons in the forming and breaking of chemical bonds between atoms, with no change to the Atomic nucleus, nuclei (no change to the elements present), and can often be described by a chemical equation. Nuclear chemistry is a sub-discipline of chemistry that involves the chemical reactions of unstable and radioactive Chemical element, elements where both electronic and nuclear changes can occur. The substance (or substances) initially involved in a chemical reaction are called reagent, reactants or reagents. Chemical reactions are usually characterized by a chemical change, and they yield one or more Product (chemistry), products, which usually have properties different from the reactants. Reactions often consist of a sequence o ...
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Fractional Distillation Lab Apparatus
A fraction is one or more equal parts of something. Fraction may also refer to: * Fraction (chemistry), a quantity of a substance collected by fractionation * Fraction (floating point number), an (ambiguous) term sometimes used to specify a part of a floating point number * Fraction (politics), a subgroup within a parliamentary party * Fraction (radiation therapy), one unit of treatment of the total radiation dose of radiation therapy that is split into multiple treatment sessions * Fraction (religion), the ceremonial act of breaking the bread during Christian Communion People with the surname * Matt Fraction, a comic book author See also

* Algebraic fraction, an indicated division in which the divisor, or both dividend and divisor, are algebraic expressions ** Irrational fraction, a type of algebraic fraction * Faction (other) * ''Frazione'', a type of administrative division of an Italian ''commune'' * Free and Independent Fraction, a Romanian political party * Par ...
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Heating Mantle
A heating mantle, or isomantle, is a piece of laboratory equipment used to apply heat to containers, as an alternative to other forms of heated bath. In contrast to other heating devices, such as hotplates or Bunsen burners, glassware containers may be placed in direct contact with the heating mantle without substantially increasing the risk of the glassware shattering, because the heating element of a heating mantle is insulated from the container so as to prevent excessive temperature gradients. Heating mantles may have various forms. In a common arrangement, electric wires are embedded within a strip of fabric that can be wrapped around a flask. The current supplied to the device, and hence the temperature achieved, is regulated by a rheostat. This type of heating mantle is quite useful for maintaining an intended temperature within a separatory funnel, for example, after the contents of a reaction have been removed from a primary heat source. Another variety of heati ...
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Hot Plate
A hot plate is a portable self-contained tabletop small appliance cooktop that features one or more electric heating elements or gas burners. A hot plate can be used as a stand-alone appliance, but is often used as a substitute for one of the burners from an oven range or a kitchen stove. Hot plates are often used for food preparation, generally in locations where a full kitchen stove would not be convenient or practical. They can also be used as a heat source in laboratories. A hot plate can have a flat surface or round surface. Hot plates can be used for traveling or in areas without electricity. Description This type of cooking equipment is typically powered by electricity; however, gas fired hot plates were not uncommon in the 19th and 20th century and are still available in various markets around the world. In scientific research In laboratory settings, hot plates are generally used to heat glassware or its contents. Some hot plates also contain an integrated magne ...
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Sand Bath
A sand bath is a common piece of laboratory equipment made from a container filled with heated sand. It is used to evenly heat another container, most often during a chemical reaction. A sand bath is most commonly used in conjunction with a hot plate or heating mantle. A beaker is filled with sand or metal pellets (called shot) and is placed on the plate or mantle. The reaction vessel is then partially covered by sand or pellets. The sand or shot then conducts the heat from the plate to all sides of the reaction vessel. This technique allows a reaction vessel to be heated throughout with minimal stirring, as opposed to heating the bottom of the vessel and waiting for convection to heat the remainder, cutting down on both the duration of the reaction and the possibility of side reactions that may occur at higher temperatures. A variation on this theme is the water bath in which the sand is replaced with water. It can be used to keep a reaction vessel at the temperature of ...
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Oil Bath
An oil bath is a type of heated bath used in a laboratory, most commonly used to heat up chemical reactions. It's essentially a container of oil that is heated by a hot plate or (in rare cases) a Bunsen burner. Use These baths are commonly used to heat reaction mixtures more evenly than would be possible with a hot plate alone, as the entire outside of the reaction flask is heated. Generally, silicone oil is used in modern oil baths, although mineral oil, cottonseed oil and even phosphoric acid have been used in the past. Hazards Overheating the oil bath can result in a fire hazard, especially if mineral oil is being used. Generally, the maximum safe operating temperature of a mineral oil bath is approximately , the oil's flash point. Mineral oil can't be used above due to the compound's boiling point. If higher temperatures are needed, a silicone oil or a sand bath may be used instead. Silicone oil baths are effective in the 25 °C (77 °F) - 230 °C (446 °F) range. Sand b ...
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Bunsen Burner
A Bunsen burner, named after Robert Bunsen, is a kind of ambient air gas burner used as laboratory equipment; it produces a single open gas flame, and is used for heating, sterilization, and combustion. The gas can be natural gas (which is mainly methane) or a liquefied petroleum gas, such as propane, butane, or a mixture. Combustion temperature achieved depends in part on the adiabatic flame temperature of the chosen fuel mixture. History In 1852, the University of Heidelberg hired Bunsen and promised him a new laboratory building. The city of Heidelberg had begun to install coal-gas street lighting, and so the university laid gas lines to the new laboratory. The designers of the building intended to use the gas not just for illumination, but also in burners for laboratory operations. For any burner lamp, it was desirable to maximize the temperature and minimize luminosity. However, existing laboratory burner lamps left much to be desired not just in terms of the heat of ...
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Flammable
A combustible material is something that can burn (i.e., ''combust'') in air. A combustible material is flammable if it ignites easily at ambient temperatures. In other words, a combustible material ignites with some effort and a flammable material catches fire immediately on exposure to flame. The degree of flammability or combustibility in air depends largely upon the volatility of the material - this is related to its composition-specific vapour pressure, which is temperature dependent. The quantity of vapour produced can be enhanced by increasing the surface area of the material forming a mist or dust. Take wood as an example. Finely divided wood dust can undergo explosive combustion and produce a blast wave. A piece of paper (made from wood) catches on fire quite easily. A heavy oak desk is much harder to ignite, even though the wood fibre is the same in all three materials. Common sense (and indeed scientific consensus until the mid-1700s) would seem to suggest that ma ...
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Laboratory Water Bath
A water bath is laboratory equipment made from a container filled with heated water. It is used to incubate samples in water at a constant temperature over a long period of time. Most water baths have a digital or an analogue interface to allow users to set a desired temperature, but some water baths have their temperature controlled by a current passing through a reader. Utilisations include warming of reagents, melting of substrates or incubation of cell cultures. It is also used to enable certain chemical reactions to occur at high temperature. Water baths are preferred heat sources for heating flammable chemicals, as their lack of open flame prevents ignition. Different types of water baths are used depending on application. For all water baths, it can be used up to 99.9 °C. When temperature is above 100 °C, alternative methods such as oil bath, silicone bath or sand bath may be used. Precautions * Use with caution. * It is not recommended to use water bath w ...
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Boiling Point
The boiling point of a substance is the temperature at which the vapor pressure of a liquid equals the pressure surrounding the liquid and the liquid changes into a vapor. The boiling point of a liquid varies depending upon the surrounding environmental pressure. A liquid in a partial vacuum has a lower boiling point than when that liquid is at atmospheric pressure. A liquid at low pressure has a lower boiling point than when that liquid is at atmospheric pressure. Because of this, water boils at under standard pressure at sea level, but at at altitude. For a given pressure, different liquids will boil at different temperatures. The normal boiling point (also called the atmospheric boiling point or the atmospheric pressure boiling point) of a liquid is the special case in which the vapor pressure of the liquid equals the defined atmospheric pressure at sea level, one atmosphere. At that temperature, the vapor pressure of the liquid becomes sufficient to overcome atmosphe ...
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Boiling
Boiling is the rapid vaporization of a liquid, which occurs when a liquid is heated to its boiling point, the temperature at which the vapour pressure of the liquid is equal to the pressure exerted on the liquid by the surrounding atmosphere. There are two main types of boiling: nucleate boiling where small bubbles of vapour form at discrete points, and critical heat flux boiling where the boiling surface is heated above a certain critical temperature and a film of vapor forms on the surface. Transition boiling is an intermediate, unstable form of boiling with elements of both types. The boiling point of water is 100 °C or 212 °F but is lower with the decreased atmospheric pressure found at higher altitudes. Boiling water is used as a method of making it potable by killing microbes and viruses that may be present. The sensitivity of different micro-organisms to heat varies, but if water is held at for one minute, most micro-organisms and viruses are inactivated. Ten mi ...
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