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Particle-induced Gamma Emission
Particle-induced gamma emission (PIGE) is a form of nuclear reaction analysis, one of the ion beam analysis thin-film analytical techniques. Technology Typically, an MeV proton beam is directed onto a sample which may be tens of microns thick, and the fast protons may excite the target nuclei such that gamma rays are emitted. These may be used to characterise the sample. For example, sodium in glass is of great importance but can be hard to measure non destructively: X-ray fluorescence (XRF) and particle-induced X-ray emission (PIXE) are both sensitive only to the surface few microns of the sample because of the low energy (and consequent high absorption coefficient) of the Na K X-rays (1.05 keV). But, for example, the 23Na(p,p'γ)23Na reaction has a high and relatively well-known cross-sectionsee the IAEA "IBANDL" site and is therefore frequently used for determining bulk sodium content of glasses, since the gamma energy (440 keV) is so high that there is effectively no a ...
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Nuclear Reaction Analysis
Nuclear may refer to: Physics Relating to the nucleus of the atom: * Nuclear engineering *Nuclear physics *Nuclear power *Nuclear reactor *Nuclear weapon *Nuclear medicine *Radiation therapy *Nuclear warfare Mathematics *Nuclear space *Nuclear operator *Nuclear congruence *Nuclear C*-algebra Biology Relating to the nucleus of the cell: * Nuclear DNA Society * Nuclear family, a family consisting of a pair of adults and their children Music * "Nuclear" (band), group music. * "Nuclear" (Ryan Adams song), 2002 *"Nuclear", a song by Mike Oldfield from his ''Man on the Rocks'' album * ''Nu.Clear'' (EP) by South Korean girl group CLC See also *Nucleus (other) *Nucleolus * Nucleation * Nucleic acid *Nucular ''Nucular'' is a common, proscribed pronunciation of the word "nuclear". It is a rough phonetic spelling of . The ''Oxford English Dictionary''s entry dates the word's first published appearance to 1943. Dictionary notes This is one of two con ...
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Ion Beam Analysis
Ion beam analysis ("IBA") is an important family of modern analytical techniques involving the use of MeV ion beams to probe the composition and obtain elemental depth profiles in the near-surface layer of solids. All IBA methods are highly sensitive and allow the detection of elements in the sub-monolayer range. The depth resolution is typically in the range of a few nanometers to a few ten nanometers. Atomic depth resolution can be achieved, but requires special equipment. The analyzed depth ranges from a few ten nanometers to a few ten micrometers. IBA methods are always quantitative with an accuracy of a few percent. Channeling allows to determine the depth profile of damage in single crystals. *RBS: Rutherford backscattering is sensitive to heavy elements in a light matrix *EBS: ''Elastic (non-Rutherford) backscattering spectrometry'' can be sensitive even to light elements in a heavy matrix. The term ''EBS'' is used when the incident particle is going so fast that it exceeds ...
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Analytical Technique
Analytical technique is a method used to determine a chemical or physical property of a chemical substance, chemical element, or mixture. There is a wide variety of techniques used for analysis, from simple weighing to advanced techniques using highly specialized instrumentation. Classical methods of analysis Classical analysis methods involve basic analytical methods widely used in laboratories. Gravimetric analysis measures the weight of the sample. Titration, Titrimetry is a technique used to determine the concentration of the analyte. Spectrochemical analysis Spectrometer can determine chemical composition through its measure of spectrums. The common spectrometer used in analytical chemistry is Mass spectrometry. In a mass spectrometer, a small amount of sample is ionized and converted to gaseous ions, where they are separated and analyzed according to their Mass-to-charge ratio, mass-to-charge ratios. Electroanalytical analysis Electroanalytical method, Electroanalytical ...
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X-ray Fluorescence
X-ray fluorescence (XRF) is the emission of characteristic "secondary" (or fluorescent) X-rays from a material that has been excited by being bombarded with high-energy X-rays or gamma rays. The phenomenon is widely used for elemental analysis and analytical chemistry, chemical analysis, particularly in the investigation of metals, glass, ceramics and building materials, and for research in geochemistry, forensic science, archaeology and art objects such as paintings. Underlying physics When materials are exposed to short-wavelength X-rays or to gamma rays, ionization of their component atoms may take place. Ionization consists of the ejection of one or more electrons from the atom, and may occur if the atom is exposed to radiation with an energy greater than its ionization energy. X-rays and gamma rays can be energetic enough to expel tightly held electrons from the inner atomic orbital, orbitals of the atom. The removal of an electron in this way makes the electronic structu ...
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Particle-induced X-ray Emission
Particle-induced X-ray emission or proton-induced X-ray emission (PIXE) is a technique used for determining the elemental composition of a material or a sample. When a material is exposed to an ion beam, atomic interactions occur that give off EM radiation of wavelengths in the x-ray part of the electromagnetic spectrum specific to an element. PIXE is a powerful yet non-destructive elemental analysis technique now used routinely by geologists, archaeologists, art conservators and others to help answer questions of provenance, dating and authenticity. The technique was first proposed in 1970 by Sven Johansson of Lund University, Sweden, and developed over the next few years with his colleagues Roland Akselsson and Thomas B Johansson. Recent extensions of PIXE using tightly focused beams (down to 1 μm) gives the additional capability of microscopic analysis. This technique, called microPIXE, can be used to determine the distribution of trace elements in a wide range of samples. A r ...
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IAEA
The International Atomic Energy Agency (IAEA) is an intergovernmental organization that seeks to promote the peaceful use of nuclear energy and to inhibit its use for any military purpose, including nuclear weapons. It was established in 1957 as an autonomous organization within the United Nations system; though governed by its own founding treaty, the organization reports to both the General Assembly and the Security Council of the United Nations, and is headquartered at the UN Office at Vienna, Austria. The IAEA was created in response to growing international concern toward nuclear weapons, especially amid rising tensions between the foremost nuclear powers, the United States and the Soviet Union. U.S. President Dwight D. Eisenhower's " Atoms for Peace" speech, which called for the creation of an international organization to monitor the global proliferation of nuclear resources and technology, is credited with catalyzing the formation of the IAEA, whose treaty came into ...
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Fluorine
Fluorine is a chemical element with the symbol F and atomic number 9. It is the lightest halogen and exists at standard conditions as a highly toxic, pale yellow diatomic gas. As the most electronegative reactive element, it is extremely reactive, as it reacts with all other elements except for the light inert gases. Among the elements, fluorine ranks 24th in universal abundance and 13th in terrestrial abundance. Fluorite, the primary mineral source of fluorine which gave the element its name, was first described in 1529; as it was added to metal ores to lower their melting points for smelting, the Latin verb meaning 'flow' gave the mineral its name. Proposed as an element in 1810, fluorine proved difficult and dangerous to separate from its compounds, and several early experimenters died or sustained injuries from their attempts. Only in 1886 did French chemist Henri Moissan isolate elemental fluorine using low-temperature electrolysis, a process still employed for modern pr ...
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Per- And Polyfluoroalkyl Substances
Per- and polyfluoroalkyl substances (PFASs) are synthetic organofluorine chemical compounds that have multiple fluorine atoms attached to an alkyl chain. An early definition, from 2011, required that they contain at least one perfluoroalkyl moiety, –CnF2n+1–. More recently (2021) the Organisation for Economic Co-operation and Development (OECD) expanded the definition, stating that "PFASs are defined as fluorinated substances that contain at least one fully fluorinated methyl or methylene carbon atom (without any H/Cl/Br/I atom attached to it), i.e. with a few noted exceptions, any chemical with at least a perfluorinated methyl group (–CF3) or a perfluorinated methylene group (–CF2–) is a PFAS." According to the OECD, at least 4,730 distinct PFASs are known with at least three perfluorinated carbon atoms. A United States Environmental Protection Agency (EPA) toxicity database, DSSTox, lists 14,735 PFASs, while PubChem lists approximately 6 million. A subgroup, the ' ...
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