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X-ray Diffraction Computed Tomography
X-ray diffraction computed tomography is an experimental technique that combines X-ray diffraction with the computed tomography data acquisition approach. X-ray diffraction (XRD) computed tomography (CT) was first introduced in 1987 by Harding et al. using a laboratory diffractometer and a monochromatic X-ray pencil beam. The first implementation of the technique at synchrotron facilities was performed in 1998 by Kleuker ''et al.'' X-ray diffraction computed tomography can be divided into two main categories depending on how the XRD data are being treated, specifically the XRD data can be treated either as powder diffraction or single crystal diffraction data and this depends on the sample properties. If the sample contains small and randomly oriented crystals, then it generates smooth powder diffraction "rings" when using a 2D area detector. If the sample contains large crystals, then it generates "spotty" 2D diffraction patterns. The latter can be performed using also a letterbo ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
X-ray Crystallography
X-ray crystallography is the experimental science of determining the atomic and molecular structure of a crystal, in which the crystalline structure causes a beam of incident X-rays to Diffraction, diffract in specific directions. By measuring the angles and intensities of the X-ray diffraction, a crystallography, crystallographer can produce a three-dimensional picture of the density of electrons within the crystal and the positions of the atoms, as well as their chemical bonds, crystallographic disorder, and other information. X-ray crystallography has been fundamental in the development of many scientific fields. In its first decades of use, this method determined the size of atoms, the lengths and types of chemical bonds, and the atomic-scale differences between various materials, especially minerals and alloys. The method has also revealed the structure and function of many biological molecules, including vitamins, drugs, proteins and nucleic acids such as DNA. X-ray crystall ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Three-dimensional X-ray Diffraction
Three-dimensional X-ray diffraction (3DXRD) is a microscopy technique using hard X-rays (with energy in the 30-100 keV range) to investigate the internal structure of polycrystalline materials in three dimensions. For a given sample, 3DXRD returns the shape, juxtaposition, and orientation of the crystallites (''"grains"'') it is made of. 3DXRD allows investigating micrometer- to millimetre-sized samples with resolution ranging from hundreds of nanometers to micrometers. Other techniques employing X-rays to investigate the internal structure of polycrystalline materials include X-ray diffraction contrast tomography (DCT) and high energy X-ray diffraction (HEDM). Compared with destructive techniques, e.g. three-dimensional electron backscatter diffraction (3D EBSD), with which the sample is serially sectioned and imaged, 3DXRD and similar X-ray nondestructive techniques have the following advantages: * They require less sample preparation, thus limiting the introduction of new struc ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Laboratory Techniques In Condensed Matter Physics
A laboratory (; ; colloquially lab) is a facility that provides controlled conditions in which scientific or technological research, experiments, and measurement may be performed. Laboratories are found in a variety of settings such as schools, universities, privately owned research institutions, corporate research and testing facilities, government regulatory and forensic investigation centers, physicians' offices, clinics, hospitals, regional and national referral centers, and even occasionally personal residences. Overview The organisation and contents of laboratories are determined by the differing requirements of the specialists working within. A physics laboratory might contain a particle accelerator or vacuum chamber, while a metallurgy laboratory could have apparatus for casting or refining metals or for testing their strength. A chemist or biologist might use a wet laboratory, while a psychologist's laboratory might be a room with one-way mirrors and hidden came ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Lattice Constant
A lattice constant or lattice parameter is one of the physical dimensions and angles that determine the geometry of the unit cells in a crystal lattice, and is proportional to the distance between atoms in the crystal. A simple cubic crystal has only one lattice constant, the distance between atoms, but, in general, lattices in three dimensions have six lattice constants: the lengths ''a'', ''b'', and ''c'' of the three cell edges meeting at a vertex, and the angles ''α'', ''β'', and ''γ'' between those edges. The crystal lattice parameters ''a'', ''b'', and ''c'' have the dimension of length. The three numbers represent the size of the unit cell, that is, the distance from a given atom to an identical atom in the same position and orientation in a neighboring cell (except for very simple crystal structures, this will not necessarily be distance to the nearest neighbor). Their SI unit is the meter, and they are traditionally specified in angstroms (Å); an angstrom being 0.1 ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Le Bail Method
Le Bail analysis is a whole diffraction pattern profile fitting technique used to characterize the properties of crystalline materials, such as structure. It was invented by Armel Le Bail around 1988. Background The Le Bail method extracts intensities (Ihkl) from powder diffraction data. This is done in order to find intensities that are suitable to determine the atomic structure of a crystalline material and to refine the unit cell and has the added advantage of checking phase-purity. Generally, the intensities of powder diffraction data are complicated by overlapping diffraction peaks with similar ''d''-spacings. For the Le Bail method, the unit cell and the approximate space group of the sample must be predetermined because they are included as a part of the fitting technique. The algorithm involves refining the unit cell, the profile parameters, and the peak intensities to match the measured powder diffraction pattern. It is not necessary to know the structural factor and as ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Rietveld Refinement
Rietveld refinement is a technique described by Hugo Rietveld for use in the characterisation of crystalline materials. The neutron diffraction, neutron and x-ray crystallography, X-ray Powder diffraction, diffraction of powder samples results in a pattern characterised by reflections (peaks in intensity) at certain positions. The height, width and position of these reflections can be used to determine many aspects of the material's structure. The Rietveld method uses a least squares approach to refine a theoretical line profile until it matches the measured profile. The introduction of this technique was a significant step forward in the diffraction analysis of powder samples as, unlike other techniques at that time, it was able to deal reliably with strongly overlapping reflections. The method was first implemented in 1967, and reported in 1969 for the diffraction of monochromatic neutrons where the reflection-position is reported in terms of the Bragg's law, Bragg angle, 2''θ' ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Voxel
In computing, a voxel is a representation of a value on a three-dimensional regular grid, akin to the two-dimensional pixel. Voxels are frequently used in the Data visualization, visualization and analysis of medical imaging, medical and scientific data (e.g. geographic information systems (GIS)). Voxels also have technical and artistic applications in video games, largely originating with surface rendering in ''Outcast (video game), Outcast'' (1999). ''Minecraft'' (2011) makes use of an entirely voxelated world to allow for a fully destructable and constructable environment. Voxel art, of the sort used in ''Minecraft'' and elsewhere, is a style and format of 3D art analogous to pixel art. As with pixels in a 2D bitmap, voxels themselves do not typically have their position (i.e. coordinates) explicitly encoded with their values. Instead, Rendering (computer graphics), rendering systems infer the position of a voxel based upon its position relative to other voxels (i.e., its pos ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Nyquist–Shannon Sampling Theorem
The Nyquist–Shannon sampling theorem is an essential principle for digital signal processing linking the frequency range of a signal and the sample rate required to avoid a type of distortion called aliasing. The theorem states that the sample rate must be at least twice the Bandwidth (signal processing), bandwidth of the signal to avoid aliasing. In practice, it is used to select band-limiting filters to keep aliasing below an acceptable amount when an analog signal is sampled or when sample rates are changed within a digital signal processing function. The Nyquist–Shannon sampling theorem is a theorem in the field of signal processing which serves as a fundamental bridge between continuous-time signals and discrete-time signals. It establishes a sufficient condition for a sample rate that permits a discrete sequence of ''samples'' to capture all the information from a continuous-time signal of finite Bandwidth (signal processing), bandwidth. Strictly speaking, the theorem ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Strain (mechanics)
In mechanics, strain is defined as relative deformation, compared to a position configuration. Different equivalent choices may be made for the expression of a strain field depending on whether it is defined with respect to the initial or the final configuration of the body and on whether the metric tensor or its dual is considered. Strain has dimension of a length ratio, with SI base units of meter per meter (m/m). Hence strains are dimensionless and are usually expressed as a decimal fraction or a percentage. Parts-per notation is also used, e.g., parts per million or parts per billion (sometimes called "microstrains" and "nanostrains", respectively), corresponding to μm/m and nm/m. Strain can be formulated as the spatial derivative of displacement: \boldsymbol \doteq \cfrac\left(\mathbf - \mathbf\right) = \boldsymbol'- \boldsymbol, where is the identity tensor. The displacement of a body may be expressed in the form , where is the reference position of material ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
CT Scan
A computed tomography scan (CT scan), formerly called computed axial tomography scan (CAT scan), is a medical imaging technique used to obtain detailed internal images of the body. The personnel that perform CT scans are called radiographers or radiology technologists. CT scanners use a rotating X-ray tube and a row of detectors placed in a gantry (medical), gantry to measure X-ray Attenuation#Radiography, attenuations by different tissues inside the body. The multiple X-ray measurements taken from different angles are then processed on a computer using tomographic reconstruction algorithms to produce Tomography, tomographic (cross-sectional) images (virtual "slices") of a body. CT scans can be used in patients with metallic implants or pacemakers, for whom magnetic resonance imaging (MRI) is Contraindication, contraindicated. Since its development in the 1970s, CT scanning has proven to be a versatile imaging technique. While CT is most prominently used in medical diagnosis, i ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Stress (mechanics)
In continuum mechanics, stress is a physical quantity that describes forces present during deformation. For example, an object being pulled apart, such as a stretched elastic band, is subject to ''tensile'' stress and may undergo elongation. An object being pushed together, such as a crumpled sponge, is subject to ''compressive'' stress and may undergo shortening. The greater the force and the smaller the cross-sectional area of the body on which it acts, the greater the stress. Stress has dimension of force per area, with SI units of newtons per square meter (N/m2) or pascal (Pa). Stress expresses the internal forces that neighbouring particles of a continuous material exert on each other, while ''strain'' is the measure of the relative deformation of the material. For example, when a solid vertical bar is supporting an overhead weight, each particle in the bar pushes on the particles immediately below it. When a liquid is in a closed container under pressure, each ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
