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Crucible
A crucible is a container in which metals or other substances may be melted or subjected to very high temperatures. Although crucibles have historically tended to be made out of clay, they can be made from any material that withstands temperatures high enough to melt or otherwise alter its contents. History Typology and chronology The form of the crucible has varied through time, with designs reflecting the process for which they are used, as well as regional variation. The earliest crucible forms derive from the sixth/fifth millennium B.C. in Eastern Europe and Iran. Chalcolithic Crucibles used for copper smelting were generally wide shallow vessels made from clay that lacks refractory properties which is similar to the types of clay used in other ceramics of the time. During the Chalcolithic period, crucibles were heated from the top by using blowpipes.Hauptmann A., 2003, ''Developments in copper Metallurgy During the Fourth and Third Millennia B.C. at Feinan'', Jordan, P ...
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Crucible Steel
Crucible steel is steel made by melting pig iron, cast iron, iron, and sometimes steel, often along with sand, glass, ashes, and other fluxes, in a crucible. Crucible steel was first developed in the middle of the 1st millennium BCE in Southern India and Sri Lanka using the wootz process. In ancient times, it was not possible to produce very high temperatures with charcoal or coal fires, which were required to melt iron or steel. However, pig iron, having a higher carbon content and thus a lower melting point, could be melted, and by soaking wrought iron or steel in the liquid pig-iron for a long time, the carbon content of the pig iron could be reduced as it slowly diffused into the iron, turning both into steel. Crucible steel of this type was produced in South and Central Asia during the medieval era. This generally produced a very hard steel, but also a composite steel that was inhomogeneous, consisting of a very high-carbon steel (formerly the pig-iron) and a lower ...
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Brass
Brass is an alloy of copper and zinc, in proportions which can be varied to achieve different colours and mechanical, electrical, acoustic and chemical properties, but copper typically has the larger proportion, generally copper and zinc. In use since prehistoric times, it is a substitutional alloy: atoms of the two constituents may replace each other within the same crystal structure. Brass is similar to bronze, a copper alloy that contains tin instead of zinc. Both bronze and brass may include small proportions of a range of other Chemical element, elements including arsenic, lead, phosphorus, aluminium, manganese and silicon. Historically, the distinction between the two alloys has been less consistent and clear, and increasingly museums use the more general term "list of copper alloys, copper alloy". Brass has long been a popular material for its bright gold-like appearance and is still used for drawer pulls and door handle, doorknobs. It has also been widely used to ma ...
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Hessian Crucible
A Hessian crucible is a type of ceramic crucible that was manufactured in the Hesse region of Germany from the late Middle Ages through the Renaissance period. They were renowned for their ability to withstand very high temperatures, rapid changes in temperature, and strong reagents. These crucibles were widely used for alchemy and early metallurgy. Millions of the vessels were exported throughout Europe, Scandinavia, and the colonies in the Americas. The crucibles were made by firing kaolinitic clay at temperatures greater than 1100°C, forming mullite. Mullite is an aluminum silicate only described in the 20th century and is responsible for the excellent properties of the Hessian crucible. Main production centre of the Hessian crucibles was the village of Großalmerode Großalmerode (; or ''Grossalmerode'') is a town in the Werra-Meißner-Kreis in Hesse, Germany. Geography Location The small town, which has had town rights since 1775, lies 21 km east of Kassel in the ...
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Wootz Steel
Wootz steel is a crucible steel characterized by a pattern of bands and high carbon content. These bands are formed by sheets of microscopic carbides within a tempered martensite or pearlite matrix in higher-carbon steel, or by ferrite and pearlite banding in lower-carbon steels. It was a pioneering steel alloy developed in southern India in the mid-1st millennium BC and exported globally. History Wootz steel originated in the mid-1st millennium BC in India, wootz steel was made in Golconda in Telangana, Karnataka, Tamilnadu and Sri Lanka. The steel was exported as cakes of steely iron that came to be known as "wootz". The method was to heat black magnetite ore in the presence of carbon in a sealed clay crucible inside a charcoal furnace to completely remove slag. An alternative was to smelt the ore first to give wrought iron, then heat and hammer it to remove slag. The carbon source was bamboo and leaves from plants such as Avārai. Locals in Sri Lanka adopted the productio ...
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Alloys
An alloy is a mixture of chemical elements of which in most cases at least one is a metallic element, although it is also sometimes used for mixtures of elements; herein only metallic alloys are described. Metallic alloys often have properties that differ from those of the pure elements from which they are made. The vast majority of metals used for commercial purposes are alloyed to improve their properties or behavior, such as increased strength, hardness or corrosion resistance. Metals may also be alloyed to reduce their overall cost, for instance alloys of gold and copper. A typical example of an alloy is 304 grade stainless steel which is commonly used for kitchen utensils, pans, knives and forks. Sometime also known as 18/8, it as an alloy consisting broadly of 74% iron, 18% chromium and 8% nickel. The chromium and nickel alloying elements add strength and hardness to the majority iron element, but their main function is to make it resistant to rust/corrosion. In an al ...
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Cementation Process
The cementation process is an Obsolescence, obsolete technology for making steel by carburization of iron. Unlike modern steelmaking, it increased the amount of carbon in the iron. It was apparently developed before the 17th century. Derwentcote Steel Furnace, built in 1720, is the earliest surviving example of a cementation furnace. Another example in the UK is the Cementation furnace, Sheffield, cementation furnace in Doncaster Street, Sheffield. Origins The process was described in a treatise published in Prague in 1574. It was invented by Johann Nussbaum of Magdeburg, who began operations at Nuremberg (with partners) in 1601. The process was patented in England by William Ellyot and Mathias Meysey in 1614. At that date, the "invention" could consist merely of the introduction of a new industry or product, or even a mere monopoly. They evidently soon transferred the patent to Sir Basil Brooke (metallurgist), Basil Brooke, but he was forced to surrender it in 1619. A cla ...
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Iron Age
The Iron Age () is the final epoch of the three historical Metal Ages, after the Chalcolithic and Bronze Age. It has also been considered as the final age of the three-age division starting with prehistory (before recorded history) and progressing to protohistory (before written history). In this usage, it is preceded by the Stone Age (subdivided into the Paleolithic, Mesolithic and Neolithic) and Bronze Age. These concepts originated for describing Iron Age Europe and the ancient Near East. In the archaeology of the Americas, a five-period system is conventionally used instead; indigenous cultures there did not develop an iron economy in the pre-Columbian era, though some did work copper and bronze. Indigenous metalworking arrived in Australia with European contact. Although meteoric iron has been used for millennia in many regions, the beginning of the Iron Age is defined locally around the world by archaeological convention when the production of Smelting, smelted iron (espe ...
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Refractory
In materials science, a refractory (or refractory material) is a material that is resistant to decomposition by heat or chemical attack and that retains its strength and rigidity at high temperatures. They are inorganic, non-metallic compounds that may be porous or non-porous, and their crystallinity varies widely: they may be crystalline, polycrystalline, amorphous, or composite. They are typically composed of oxides, carbides or nitrides of the following elements: silicon, aluminium, magnesium, calcium, boron, chromium and zirconium. Many refractories are ceramics, but some such as graphite are not, and some ceramics such as clay pottery are not considered refractory. Refractories are distinguished from the '' refractory metals'', which are elemental metals and their alloys that have high melting temperatures. Refractories are defined by ASTM C71 as "non-metallic materials having those chemical and physical properties that make them applicable for structures, o ...
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Bronze Casting
Lost-wax castingalso called investment casting, precision casting, or ''cire perdue'' (; borrowed from French)is the process by which a duplicate sculpture (often a metal, such as silver, gold, brass, or bronze) is cast from an original sculpture. Intricate works can be achieved by this method. The oldest known examples of this technique are approximately 6,500 years old (4550–4450 BC) and attributed to gold artefacts found at Bulgaria's Varna Necropolis. A copper amulet from Mehrgarh, Indus Valley civilization, in present-day Pakistan, is dated to circa 4,000 BC. Cast copper objects, found in the Nahal Mishmar hoard in southern Israel, which belong to the Chalcolithic period (4500–3500 BC), are estimated, from carbon-14 dating, to date to circa 3500 BC. Other examples from somewhat later periods are from Mesopotamia in the third millennium BC. Lost-wax casting was widespread in Europe until the 18th century, when a piece-moulding process came to predominate. The steps ...
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Cupellation
Cupellation is a refining process in metallurgy in which ores or alloyed metals are treated under very high temperatures and subjected to controlled operations to separate noble metals, like gold and silver, from base metals, like lead, copper, zinc, arsenic, antimony, or bismuth, present in the ore. The process is based on the principle that precious metals typically oxidise or react chemically at much higher temperatures than base metals. When they are heated at high temperatures, the precious metals remain apart, and the others react, forming slags or other compounds.Bayley, J. 2008 Since the Early Bronze Age, the process was used to obtain silver from smelted lead ores.Rehren, Th., Eckstein, K. 2002 By the Middle Ages and the Renaissance, cupellation was one of the most common processes for refining precious metals. By then, fire assays were used for assaying minerals: testing fresh metals such as lead and recycled metals to determine their purity for jewellery ...
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Medieval Era
In the history of Europe, the Middle Ages or medieval period lasted approximately from the 5th to the late 15th centuries, similarly to the post-classical period of global history. It began with the fall of the Western Roman Empire and transitioned into the Renaissance and the Age of Discovery. The Middle Ages is the middle period of the three traditional divisions of Western history: classical antiquity, the medieval period, and the modern period. The medieval period is itself subdivided into the Early, High, and Late Middle Ages. Population decline, counterurbanisation, the collapse of centralised authority, invasions, and mass migrations of tribes, which had begun in late antiquity, continued into the Early Middle Ages. The large-scale movements of the Migration Period, including various Germanic peoples, formed new kingdoms in what remained of the Western Roman Empire. In the 7th century, North Africa and the Middle East—once part of the Byzantine Empire—came un ...
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Hesse
Hesse or Hessen ( ), officially the State of Hesse (), is a States of Germany, state in Germany. Its capital city is Wiesbaden, and the largest urban area is Frankfurt, which is also the country's principal financial centre. Two other major historic cities are Darmstadt and Kassel. With an area of 21,114.73 square kilometers and a population of over six million, it ranks seventh and fifth, respectively, among the sixteen German states. Frankfurt Rhine-Main, Germany's second-largest metropolitan area (after Rhine-Ruhr), is mainly located in Hesse. As a cultural region, Hesse also includes the area known as Rhenish Hesse (Rheinhessen) in the neighboring state of Rhineland-Palatinate. Etymology The German name , like the names of other German regions ( "Swabia", "Franconia", "Bavaria", "Saxony"), derives from the dative plural form of the name of the inhabitants or German tribes, eponymous tribe, the Hessians (, singular ). The geographical name represents a short equivalent o ...
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