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Siwoloboff Method
The Siwoloboff method is used to determine the boiling point of small samples of liquid chemicals. A sample in an ignition tube (also called a fusion tube) is attached to a thermometer with a rubber band, and immersed in a Thiele tube The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point of a substance. The apparatus resembl ..., water bath, or other suitable medium for heating. A sealed capillary, open end pointing down, is placed in the ignition tube. The apparatus is heated. Dissolved gases evolve from the sample first, and the air in the capillary tube expands. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample. References Laboratory techniques {{Analytical chemi ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Siwoloboff Method
The Siwoloboff method is used to determine the boiling point of small samples of liquid chemicals. A sample in an ignition tube (also called a fusion tube) is attached to a thermometer with a rubber band, and immersed in a Thiele tube The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point of a substance. The apparatus resembl ..., water bath, or other suitable medium for heating. A sealed capillary, open end pointing down, is placed in the ignition tube. The apparatus is heated. Dissolved gases evolve from the sample first, and the air in the capillary tube expands. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample. References Laboratory techniques {{Analytical chemi ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Test Tube
A test tube, also known as a culture tube or sample tube, is a common piece of laboratory glassware consisting of a finger-like length of glass or clear plastic tubing, open at the top and closed at the bottom. Test tubes are usually placed in special-purpose test tube rack, racks. Types and usage Chemistry Test tubes intended for general chemical work are usually made of glass, for its relative resistance to heat. Tubes made from expansion-resistant glasses, mostly borosilicate glass or fused quartz, can withstand high temperatures up to several hundred degrees Celsius. Chemistry tubes are available in a multitude of lengths and widths, typically from 10 to 20 mm wide and 50 to 200 mm long. The top often features a flared lip to aid pouring out the contents. A chemistry test tube typically has a flat bottom, a round bottom, or a conical bottom. Some test tubes are made to accept a ground glass joint, ground glass stopper or a screw cap. They are often provided w ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Thiele Tube
The Thiele tube, named after the German chemist Johannes Thiele, is a laboratory glassware designed to contain and heat an oil bath. Such a setup is commonly used in the determination of the melting point of a substance. The apparatus resembles a glass test tube with an attached handle. Operation Oil is poured into the tube, and then the "handle" is heated, either by a small flame or some other heating element. The shape of the Thiele tube allows for formation of convection currents in the oil when it is heated. These currents maintain a fairly uniform temperature distribution throughout the oil in the tube. The side arm of the tube is designed to generate these convection currents and thus transfer the heat from the flame evenly and rapidly throughout the heating oil. The sample, packed in a capillary tube, is attached to the thermometer, and held by means of a rubber band or a small slice of rubber tubing. The Thiele tube is usually heated using a microburner ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
University Of Calgary
The University of Calgary (U of C or UCalgary) is a public research university located in Calgary, Alberta, Canada. The University of Calgary started in 1944 as the Calgary branch of the University of Alberta, founded in 1908, prior to being instituted into a separate, autonomous university in 1966. It is composed of 14 faculties and over 85 research institutes and centres. The main campus is located in the northwest quadrant of the city near the Bow River and a smaller south campus is located in the city centre. The main campus houses most of the research facilities and works with provincial and federal research and regulatory agencies, several of which are housed next to the campus such as the Geological Survey of Canada. The main campus covers approximately . A member of the U15, the University of Calgary is also one of Canada's top research universities (based on the number of Canada Research Chairs). The university has a sponsored research revenue of $380.4 million, wi ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
