Desiccator
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Desiccator
Desiccators are sealable enclosures containing desiccants used for preserving moisture-sensitive items such as cobalt chloride paper for another use. A common use for desiccators is to protect chemicals which are hygroscopic or which react with water from humidity. The contents of desiccators are exposed to atmospheric moisture whenever the desiccators are opened. It also requires some time to achieve a low humidity. Hence they are not appropriate for storing chemicals which react quickly or violently with atmospheric moisture such as the alkali metals; a glovebox or Schlenk-type apparatus may be more suitable for these purposes. Desiccators are sometimes used to remove traces of water from an almost-dry sample. Where a desiccator alone is unsatisfactory, the sample may be dried at elevated temperature using Abderhalden's drying pistol. Constituents The lower compartment of the desiccator contains lumps of silica gel, freshly calcined quicklime, Drierite or (not as effective) ...
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Desiccator
Desiccators are sealable enclosures containing desiccants used for preserving moisture-sensitive items such as cobalt chloride paper for another use. A common use for desiccators is to protect chemicals which are hygroscopic or which react with water from humidity. The contents of desiccators are exposed to atmospheric moisture whenever the desiccators are opened. It also requires some time to achieve a low humidity. Hence they are not appropriate for storing chemicals which react quickly or violently with atmospheric moisture such as the alkali metals; a glovebox or Schlenk-type apparatus may be more suitable for these purposes. Desiccators are sometimes used to remove traces of water from an almost-dry sample. Where a desiccator alone is unsatisfactory, the sample may be dried at elevated temperature using Abderhalden's drying pistol. Constituents The lower compartment of the desiccator contains lumps of silica gel, freshly calcined quicklime, Drierite or (not as effective) ...
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Desiccation
Desiccation () is the state of extreme dryness, or the process of extreme drying. A desiccant is a hygroscopic (attracts and holds water) substance that induces or sustains such a state in its local vicinity in a moderately sealed container. Industry Desiccation is widely employed in the oil and gas industry. These materials are obtained in a hydrated state, but the water content leads to corrosion or is incompatible with downstream processing. Removal of water is achieved by cryogenic condensation, absorption into glycols, and absorption onto desiccants such as silica gel. Laboratory A desiccator is a heavy glass or plastic container, now somewhat antiquated, used in practical chemistry for drying or keeping small amounts of materials very dry. The material is placed on a shelf, and a drying agent or ''desiccant'', such as dry silica gel or anhydrous sodium hydroxide, is placed below the shelf. Often some sort of humidity indicator is included in the desiccator to show, ...
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Abderhalden's Drying Pistol
Abderhalden's drying pistol is a piece of laboratory glassware used to free samples from traces of water, or other impurities. It is called a "pistol" because of its resemblance to the firearm. Its use has declined due to modern hotplate technology and vacuum pumps. The apparatus was first described in a book edited by Emil Abderhalden. The drying pistol allows the sample to be dried at elevated temperature; this is especially preferred when storage in a desiccator at room temperature does not give satisfactory results. Operation The drying pistol consists of two concentric barrels; the inner is connected to a vacuum source via a trap. The outer barrel is connected at the bottom to a round bottom flask, and a condenser. To operate the drying pistol, a sample is placed within the inner barrel, and the barrel is evacuated. The round bottom flask, filled with an appropriate solvent, is heated to a boil. Hot vapors warm the inner barrel; losses are avoided with the condenser. By choos ...
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Calcium Sulfate
Calcium sulfate (or calcium sulphate) is the inorganic compound with the formula CaSO4 and related hydrates. In the form of γ-anhydrite (the anhydrous form), it is used as a desiccant. One particular hydrate is better known as plaster of Paris, and another occurs naturally as the mineral gypsum. It has many uses in industry. All forms are white solids that are poorly soluble in water.Franz Wirsching "Calcium Sulfate" in Ullmann's Encyclopedia of Industrial Chemistry, 2012 Wiley-VCH, Weinheim. Calcium sulfate causes permanent hardness in water. Hydration states and crystallographic structures The compound exists in three levels of hydration corresponding to different crystallographic structures and to minerals: * (anhydrite): anhydrous state. The structure is related to that of zirconium orthosilicate (zircon): is 8-coordinate, is tetrahedral, O is 3-coordinate. * (gypsum and selenite (mineral)): dihydrate. * (bassanite): hemihydrate, also known as plaster of Paris. S ...
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Bell Jar
A bell jar is a glass jar, similar in shape to a bell (i.e. in its best-known form it is open at the bottom, while its top and sides together are a single piece), and can be manufactured from a variety of materials (ranging from glass to different types of metals). Bell jars are often used in laboratories to form and contain a vacuum. It is a common science apparatus used in experiments. Bell jars have a limited ability to create strong vacuums; vacuum chambers are available when higher performance is needed. They have been used to demonstrate the effect of vacuum on sound propagation. In addition to their scientific applications, bell jars may also serve as display cases or transparent dust covers. In these situations the bell jar is not usually placed under vacuum. Vacuum A vacuum bell jar is placed on a base which is vented to a hose fitting, that can be connected via a hose to a vacuum pump. A vacuum is formed by pumping the air out of the bell jar. The lower edge of a va ...
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Flange
A flange is a protruded ridge, lip or rim (wheel), rim, either external or internal, that serves to increase shear strength, strength (as the flange of an iron beam (structure), beam such as an I-beam or a T-beam); for easy attachment/transfer of contact force with another object (as the flange on the end of a pipe (fluid conveyance), pipe, steam cylinder, etc., or on the lens mount of a camera); or for stabilizing and guiding the movements of a machine or its parts (as the inside flange of a railroad car, rail car or tram train wheel, wheel, which keep the wheels from derailment, running off the rail profile, rails). Flanges are often attached using bolts in the pattern of a bolt circle. The term "flange" is also used for a kind of tool used to form flanges. Plumbing or piping A flange can also be a plate or ring to form a rim at the end of a pipe when fastened to the pipe (for example, a closet flange). A blind flange is a plate for covering or closing the end of a pipe. A ...
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Grease (lubricant)
Grease is a solid or semisolid lubricant formed as a dispersion of thickening agents in a liquid lubricant. Grease generally consists of a soap emulsified with mineral or vegetable oil. A common feature of greases is that they possess a high initial viscosity, which upon the application of shear, drops to give the effect of an oil-lubricated bearing of approximately the same viscosity as the base oil used in the grease. This change in viscosity is called shear thinning. Grease is sometimes used to describe lubricating materials that are simply soft solids or high viscosity liquids, but these materials do not exhibit the shear-thinning properties characteristic of the classical grease. For example, petroleum jellies such as Vaseline are not generally classified as greases. Greases are applied to mechanisms that can be lubricated only infrequently and where a lubricating oil would not stay in position. They also act as sealants to prevent ingress of water and incompressible materia ...
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Implosion (mechanical Process)
Implosion is a process in which objects are destroyed by collapsing (or being squeezed in) on themselves. The opposite of explosion (which expands the volume), implosion reduces the volume occupied and concentrates matter and energy. True implosion usually involves a difference between internal (lower) and external (higher) pressure, or inward and outward forces, that is so large that the structure collapses inward into itself, or into the space it occupied if it is not a completely solid object. Examples of implosion include a submarine being crushed from the outside by the hydrostatic pressure of the surrounding water, and the collapse of a massive star under its own gravitational pressure. An implosion ''can'' propel material outward (for example due to the force of inward falling material rebounding, or peripheral material being ejected as the inner parts collapse), but this is not an essential component of an implosion and not all kinds of implosion will do so. If the obje ...
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Stopcock
A stopcock is a form of valve used to control the flow of a liquid or gas. The term is not precise and is applied to many different types of valve. The only consistent attribute is that the valve is designed to completely stop the flow when closed fully. Use Water service Stopcocks are used to grossly regulate the flow of tap water in residential and commercial services. One is found at the junction of a water main and the branch leading to an individual service (allowing the service to be isolated from the main trunk), and a second inside the structure (allowing its plumbing to be isolated from the branch line leading into it). Either is employed when maintenance or emergency repairs are conducted. Laboratory For laboratory glassware, items sometimes have plug valves with conically-tapered inserts called stopcocks (sometimes referred to as "plugs" by laypeople) with different bores. The valve bodies are usually made of glass, while the plugs are made of glass or Teflon. O ...
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Glass
Glass is a non-crystalline, often transparent, amorphous solid that has widespread practical, technological, and decorative use in, for example, window panes, tableware, and optics. Glass is most often formed by rapid cooling (quenching) of the molten form; some glasses such as volcanic glass are naturally occurring. The most familiar, and historically the oldest, types of manufactured glass are "silicate glasses" based on the chemical compound silica (silicon dioxide, or quartz), the primary constituent of sand. Soda–lime glass, containing around 70% silica, accounts for around 90% of manufactured glass. The term ''glass'', in popular usage, is often used to refer only to this type of material, although silica-free glasses often have desirable properties for applications in modern communications technology. Some objects, such as drinking glasses and eyeglasses, are so commonly made of silicate-based glass that they are simply called by the name of the material. Despite bei ...
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Calcium Chloride
Calcium chloride is an inorganic compound, a salt with the chemical formula . It is a white crystalline solid at room temperature, and it is highly soluble in water. It can be created by neutralising hydrochloric acid with calcium hydroxide. Calcium chloride is commonly encountered as a hydrated solid with generic formula , where ''n'' = 0, 1, 2, 4, and 6. These compounds are mainly used for de-icing and dust control. Because the anhydrous salt is hydroscopic and deliquescent, it is used as a desiccant.Robert Kemp, Suzanne E. Keegan "Calcium Chloride" in Ullmann's Encyclopedia of Industrial Chemistry 2000, Wiley-VCH, Weinheim. Uses De-icing and freezing-point depression By depressing the freezing point of water, calcium chloride is used to prevent ice formation and is used to de-ice. This application consumes the greatest amount of calcium chloride. Calcium chloride is relatively harmless to plants and soil. As a deicing agent, it is much more effective at lower temperat ...
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Quicklime
Calcium oxide (CaO), commonly known as quicklime or burnt lime, is a widely used chemical compound. It is a white, caustic, alkaline, crystalline solid at room temperature. The broadly used term "''lime''" connotes calcium-containing inorganic materials, in which carbonates, oxides and hydroxides of calcium, silicon, magnesium, aluminium, and iron predominate. By contrast, ''quicklime'' specifically applies to the single chemical compound calcium oxide. Calcium oxide that survives processing without reacting in building products such as cement is called free lime. Quicklime is relatively inexpensive. Both it and a chemical derivative ( calcium hydroxide, of which quicklime is the base anhydride) are important commodity chemicals. Preparation Calcium oxide is usually made by the thermal decomposition of materials, such as limestone or seashells, that contain calcium carbonate (CaCO3; mineral calcite) in a lime kiln. This is accomplished by heating the material to above ,Merck ...
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