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Gooch Crucible
{{Short description, Gooch crucible A Gooch crucible, named after Frank Austin Gooch,Classic Kit: Gooch's Cruciblby Dr. Andrea Sella is a filtration device for laboratory use (and was also called a Gooch filterJ. Am. Chem. Soc., 1882, 4 (8), p 161). It is convenient for collecting a precipitate directly within the vessel in which it is to be dried, possibly Ash (analytical chemistry), ashed, and finally weighed in gravimetric analysis. The device was originally a standard platinum laboratory crucible with a perforated base into which asbestos pulp was placed to form the filter mat. The crucible was then heated in an oven to dry out until it attained constant weight. The use of these materials meant that after filtration, the crucible and its contents could be subjected to high temperature to dry the filtrate and possibly oxidize or ash it to minimum weight. However, because of the high cost of platinum, versions made of porcelain were introduced in 1882. ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Frank Austin Gooch
Frank Austin Gooch (1852 – 1929) was a chemist and engineer. Biography He was born to Joshua G. & Sarah Gates (Coolidge) Gooch in Watertown, Massachusetts. On his mother's side of the family, he was a descendant of Thomas Hastings (colonist) who came from the East Anglia region of England to the Massachusetts Bay Colony in 1634.Buckminster, Lydia N.H., The Hastings Memorial, A Genealogical Account of the Descendants of Thomas Hastings of Watertown, Mass. from 1634 to 1864, Boston: Samuel G. Drake Publisher (an undated NEHGS photoduplicate of the 1866 edition), 126. Gooch invented the Gooch crucible, which is used, for example, to determine the solubility of bituminous materials such as road tars and petroleum asphalts. He was awarded a Ph.D. by Harvard University in 1877. Gooch was a Professor of Chemistry at Yale University from 1885 to 1918. He devised or perfected a large number of analytical processes and methods, including: * Invented the Gooch crucible, Gooch filt ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Ash (analytical Chemistry)
In analytical chemistry, ashing or ash content determination is the process of mineralization for preconcentration of trace substances prior to a chemical analysis, such as chromatography, or optical analysis, such as spectroscopy. Overview The ash content of a sample is a measure of the amount of inorganic noncombustible material it contains. The residues after a sample is completely burnt - in contrast to the ash remaining after incomplete combustion - typically consist of oxides of the inorganic elements present in the original sample. Ash is one of the components in the proximate analysis of biological materials, consisting mainly of salty, inorganic constituents. It includes metal salts which are important for processes requiring ions such as Na+ (Sodium), K+ (Potassium), and Ca2+ (Calcium). It also includes trace minerals which are required for unique molecules, such as chlorophyll and hemoglobin. Procedures for ash content determination are similar to procedures for Loss ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Gravimetric Analysis
Gravimetric analysis describes a set of methods used in analytical chemistry for the quantitative determination of an analyte (the ion being analyzed) based on its mass. The principle of this type of analysis is that once an ion's mass has been determined as a unique compound, that known measurement can then be used to determine the same analyte's mass in a mixture, as long as the relative quantities of the other constituents are known. The four main types of this method of analysis are ''precipitation'', ''volatilization'', ''electro-analytical'' and ''miscellaneous physical method''. The methods involve changing the phase of the analyte to separate it in its pure form from the original mixture and are quantitative measurements. Precipitation method The precipitation method is the one used for the determination of the amount of calcium in water. Using this method, an excess of oxalic acid, H2C2O4, is added to a measured, known volume of water. By adding a reagent, here ammoni ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Platinum
Platinum is a chemical element with the symbol Pt and atomic number 78. It is a dense, malleable, ductile, highly unreactive, precious, silverish-white transition metal. Its name originates from Spanish , a diminutive of "silver". Platinum is a member of the platinum group of elements and group 10 of the periodic table of elements. It has six naturally occurring isotopes. It is one of the rarer elements in Earth's crust, with an average abundance of approximately 5 μg/kg. It occurs in some nickel and copper ores along with some native deposits, mostly in South Africa, which accounts for ~80% of the world production. Because of its scarcity in Earth's crust, only a few hundred tonnes are produced annually, and given its important uses, it is highly valuable and is a major precious metal commodity. Platinum is one of the least reactive metals. It has remarkable resistance to corrosion, even at high temperatures, and is therefore considered a noble metal. Consequent ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Asbestos
Asbestos () is a naturally occurring fibrous silicate mineral. There are six types, all of which are composed of long and thin fibrous crystals, each fibre being composed of many microscopic "fibrils" that can be released into the atmosphere by abrasion and other processes. Inhalation of asbestos fibres can lead to various dangerous lung conditions, including mesothelioma, asbestosis, and lung cancer, so it is now notorious as a serious health and safety hazard. Archaeological studies have found evidence of asbestos being used as far back as the Stone Age to strengthen ceramic pots, but large-scale mining began at the end of the 19th century when manufacturers and builders began using asbestos for its desirable physical properties. Asbestos is an excellent electrical insulator and is highly fire-resistant, so for much of the 20th century it was very commonly used across the world as a building material, until its adverse effects on human health were more widely acknowledged ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Porcelain
Porcelain () is a ceramic material made by heating substances, generally including materials such as kaolinite, in a kiln to temperatures between . The strength and translucence of porcelain, relative to other types of pottery, arises mainly from vitrification and formation of the mineral mullite within the body at these high temperatures. Though definitions vary, porcelain can be divided into three main categories: hard-paste, soft-paste, and bone china. The category that an object belongs to depends on the composition of the paste used to make the body of the porcelain object and the firing conditions. Porcelain slowly evolved in China and was finally achieved (depending on the definition used) at some point about 2,000 to 1,200 years ago; it slowly spread to other East Asian countries, then to Europe, and eventually to the rest of the world. Its manufacturing process is more demanding than that for earthenware and stoneware, the two other main types of pottery, and it ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Aspirator (pump)
A vacuum ejector, or simply ejector is a type of vacuum pump, which produces vacuum by means of the Venturi effect. In an ejector, a working fluid (liquid or gaseous) flows through a jet nozzle into a tube that first narrows and then expands in cross-sectional area. The fluid leaving the jet is flowing at a high velocity which due to Bernoulli's principle results in it having low pressure, thus generating a vacuum. The outer tube then narrows into a mixing section where the high velocity working fluid mixes with the fluid that is drawn in by the vacuum, imparting enough velocity for it to be ejected, the tube then typically expands in order to decrease the velocity of the ejected stream, allowing the pressure to smoothly increase to the external pressure. The strength of the vacuum produced depends on the velocity and shape of the fluid jet and the shape of the constriction and mixing sections, but if a liquid is used as the working fluid the strength of the vacuum produced is l ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Büchner Flask
A Büchner flask, also known as a vacuum flask,The use of the term ''vacuum flask'' sometimes causes confusion with the Thermos flask filter flask, suction flask, side-arm flask, Kitasato flask or Bunsen flask, is a thick-walled Erlenmeyer flask with a short glass tube and hose barb protruding about an inch from its neck. The short tube and hose barb effectively act as an adapter over which the end of a thick-walled flexible hose (tubing) can be fitted to form a connection to the flask. The other end of the hose can be connected to source of vacuum such as an aspirator, vacuum pump, or house vacuum. Preferably this is done through a trap (see below), which is designed to prevent the sucking back of water from the aspirator into the Büchner flask. The purpose of applying a vacuum is to speed the filtration by providing a pressure differential across the filter medium that is greater than that produced by gravity alone. The thick wall of the Büchner flask provides it the stren ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
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