Powder mill
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A powder mill was a mill where
gunpowder Gunpowder, also commonly known as black powder to distinguish it from modern smokeless powder, is the earliest known chemical explosive. It consists of a mixture of sulfur, carbon (in the form of charcoal) and potassium nitrate (saltpeter). T ...
is made from
sulfur Sulfur (or sulphur in British English) is a chemical element with the symbol S and atomic number 16. It is abundant, multivalent and nonmetallic. Under normal conditions, sulfur atoms form cyclic octatomic molecules with a chemical formul ...
,
saltpeter Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate Salt (chemistry), salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ...
and
charcoal Charcoal is a lightweight black carbon residue produced by strongly heating wood (or other animal and plant materials) in minimal oxygen to remove all water and volatile constituents. In the traditional version of this pyrolysis process, ...
.


Milling steps

Crude grinding and mixing operations such as the Frankford Powder-Mill of
Philadelphia Philadelphia, often called Philly, is the largest city in the Commonwealth of Pennsylvania, the sixth-largest city in the U.S., the second-largest city in both the Northeast megalopolis and Mid-Atlantic regions after New York City. Since ...
were a
cottage industry The putting-out system is a means of subcontracting work. Historically, it was also known as the workshop system and the domestic system. In putting-out, work is contracted by a central agent to subcontractors who complete the project via remote ...
until the
industrial revolution The Industrial Revolution was the transition to new manufacturing processes in Great Britain, continental Europe, and the United States, that occurred during the period from around 1760 to about 1820–1840. This transition included going f ...
brought improved product quality through the following procedures: *
Charcoal Charcoal is a lightweight black carbon residue produced by strongly heating wood (or other animal and plant materials) in minimal oxygen to remove all water and volatile constituents. In the traditional version of this pyrolysis process, ...
was often manufactured nearby from locally available trees, but the heating retorts were typically separated from the other buildings to minimize fire danger. Trees with low value as sources of
lumber Lumber is wood that has been processed into dimensional lumber, including beams and planks or boards, a stage in the process of wood production. Lumber is mainly used for construction framing, as well as finishing (floors, wall panels, w ...
were debarked, dried, and cut to uniform length to fit into iron retorts with
cast iron Cast iron is a class of iron– carbon alloys with a carbon content more than 2%. Its usefulness derives from its relatively low melting temperature. The alloy constituents affect its color when fractured: white cast iron has carbide impuri ...
doors. The retorts were carefully packed to leave as little air space as possible, and the retort doors were closed and sealed with clay to prevent entry of air as the retorts were heated by external fires. Volatile gas generated by the heating process was vented through a small flue at the top of each retort. After the external fires were extinguished, the retorts were allowed to cool before the doors were opened to remove the charcoal. * High purity
sulfur Sulfur (or sulphur in British English) is a chemical element with the symbol S and atomic number 16. It is abundant, multivalent and nonmetallic. Under normal conditions, sulfur atoms form cyclic octatomic molecules with a chemical formul ...
usually required little preparation other than grinding to a powder. Separate grinding mills reduced cool charcoal and sulfur to fine powders. * Crude
saltpeter Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate Salt (chemistry), salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ...
(KNO3) was dissolved in a pot of boiling water. After boiling, a small amount of floating glue might be added to the hot water to aid skimming off floating impurities. The hot solution was then carefully decanted to avoid suspending
insoluble In chemistry, solubility is the ability of a substance, the solute, to form a solution with another substance, the solvent. Insolubility is the opposite property, the inability of the solute to form such a solution. The extent of the solubi ...
solid impurities settled to the bottom of the pot. The hot decanted liquid was distributed into shallow wooden vats where
evaporative cooling An evaporative cooler (also known as evaporative air conditioner, swamp cooler, swamp box, desert cooler and wet air cooler) is a device that cools air through the evaporation of water. Evaporative cooling differs from other air conditioning ...
would remove excess water. Purified
potassium nitrate Potassium nitrate is a chemical compound with the chemical formula . This alkali metal nitrate salt is also known as Indian saltpetre (large deposits of which were historically mined in India). It is an ionic salt of potassium ions K+ and ...
recrystallized while the cooling solution was gently agitated with broad hoes to prevent formation of large
crystal A crystal or crystalline solid is a solid material whose constituents (such as atoms, molecules, or ions) are arranged in a highly ordered microscopic structure, forming a crystal lattice that extends in all directions. In addition, macro ...
s. * Powdered sulfur and charcoal were combined in appropriate ratios with moist saltpeter crystals, and the moist paste was mixed and compacted by kneading beneath heavy rotating wheels in a press mill. * The compressed cake was transferred to a corning mill or kernelling mill to be cut into pieces of approximately correct size by
bronze Bronze is an alloy consisting primarily of copper, commonly with about 12–12.5% tin and often with the addition of other metals (including aluminium, manganese, nickel, or zinc) and sometimes non-metals, such as phosphorus, or metalloids suc ...
- or
zinc Zinc is a chemical element with the symbol Zn and atomic number 30. Zinc is a slightly brittle metal at room temperature and has a shiny-greyish appearance when oxidation is removed. It is the first element in group 12 (IIB) of the periodi ...
-toothed wheels. * Kernelling mill products were sorted by size using leather
sieve A sieve, fine mesh strainer, or sift, is a device for separating wanted elements from unwanted material or for controlling the particle size distribution of a sample, using a screen such as a woven mesh or net or perforated sheet materia ...
s. Oversize product was returned to the kernelling mill, while undersize product was returned to the press mill. * Sorted kernels of desired size were dried and mixed with
graphite Graphite () is a crystalline form of the element carbon. It consists of stacked layers of graphene. Graphite occurs naturally and is the most stable form of carbon under standard conditions. Synthetic and natural graphite are consumed on la ...
to be tumbled in glazing mill barrels. Graphite coating reduced the tendency of grains to stick together in storage. * Glazed product was typically packaged in wooden kegs. Filled kegs were transported away from the mill as soon as possible to a powder magazine for wholesale distribution. The potential for destructive energy release from powder magazine accidents required the magazines to be distant from both the powder mill and other places of business or habitation.


Explosions

Gunpowder is very easily ignited by
static electricity Static electricity is an imbalance of electric charges within or on the surface of a material or between materials. The charge remains until it is able to move away by means of an electric current or electrical discharge. Static electricity is na ...
or
lightning strike A lightning strike or lightning bolt is an electric discharge between the atmosphere and the ground. Most originate in a cumulonimbus cloud and terminate on the ground, called cloud-to-ground (CG) lightning. A less common type of strike, ground- ...
s, and most powder mills experienced occasional accidental
explosion An explosion is a rapid expansion in volume associated with an extreme outward release of energy, usually with the generation of high temperatures and release of high-pressure gases. Supersonic explosions created by high explosives are known ...
s. Powder mill explosions typically destroyed an entire building and killed those working in the vicinity of the building. Explosions might throw flaming debris which could ignite other buildings. Successful mills were typically built as an arrangement of separate buildings to minimize the loss from any single building explosion. Buildings were separated by enough distance to minimize the risk of being damaged by an explosion in an adjacent building. Buildings were usually built of stone with one weak wooden wall and roof to direct the force and debris from an accidental explosion toward a river or an open field.


Power supply

Powder mills were originally powered by
windmill A windmill is a structure that converts wind power into rotational energy using vanes called sails or blades, specifically to mill grain (gristmills), but the term is also extended to windpumps, wind turbines, and other applications, in some ...
s, water mills or
horse mill A horse mill is a mill, sometimes used in conjunction with a watermill or windmill, that uses a horse engine as the power source. Any milling process can be powered in this way, but the most frequent use of animal power in horse mills was for g ...
s. Despite later availability of
steam engine A steam engine is a heat engine that performs mechanical work using steam as its working fluid. The steam engine uses the force produced by steam pressure to push a piston back and forth inside a cylinder. This pushing force can be ...
s, the older power sources did not require a fire to generate
steam Steam is a substance containing water in the gas phase, and sometimes also an aerosol of liquid water droplets, or air. This may occur due to evaporation or due to boiling, where heat is applied until water reaches the enthalpy of vaporizatio ...
, and avoided the possibility of sparks which might ignite the gunpowder. Some 20th-century powder mills used electric power. Before the availability of safe electrical power, some of the most successful mills were built along rivers where water could be distributed through a
power canal A Power canal refers to a canal used for hydraulic power generation, rather than for transport of watercraft. The power canal was a major factor in the Industrial revolution in New England in the 19th century. Most early power canals were mill ...
to individual buildings and intermediate products could be floated from one building to the next. The power canal offered a supply of firefighting water, and the adjacent river was a relatively safe direction to focus explosion debris. Where water transport was impractical, intermediate products were often transported in wagons pulled by
draft animal A working animal is an animal, usually domesticated, that is kept by humans and trained to perform tasks instead of being slaughtered to harvest animal products. Some are used for their physical strength (e.g. oxen and draft horses) or for ...
s. The wagons were often built entirely of wood held together with wooden pegs, and draft animals were usually unshod to avoid sparks from steel shoes or nails.


In the United States

The 1810 census reported 208 powder mills in the United States. In 1802, the
DuPont DuPont de Nemours, Inc., commonly shortened to DuPont, is an American multinational chemical company first formed in 1802 by French-American chemist and industrialist Éleuthère Irénée du Pont de Nemours. The company played a major role in ...
family started their industrial enterprises in the
United States The United States of America (U.S.A. or USA), commonly known as the United States (U.S. or US) or America, is a country Continental United States, primarily located in North America. It consists of 50 U.S. state, states, a Washington, D.C., ...
by building the
Eleutherian Mills From 1802 to 1921, Eleutherian Mills was a gunpowder mill site used for the manufacture of explosives founded by Eleuthère Irénée du Pont, which grew into the DuPont company. The name also refers to the house on the hill above the mills, whi ...
on the Brandywine Creek in
Delaware Delaware ( ) is a state in the Mid-Atlantic region of the United States, bordering Maryland to its south and west; Pennsylvania to its north; and New Jersey and the Atlantic Ocean to its east. The state takes its name from the adjacent ...
. Four mills were manufacturing 69 percent of United States gunpowder when gunpowder production peaked during the
American Civil War The American Civil War (April 12, 1861 – May 26, 1865; also known by Names of the American Civil War, other names) was a civil war in the United States. It was fought between the Union (American Civil War), Union ("the North") and t ...
. They were the DuPont mill, the
Hazard Powder Company The Hazard Powder Company is a former American manufacturer of gunpowder and explosives. It was located in Hazardville within the town of Enfield, Connecticut. History The company was founded on the Scantic River in 1835 by Allen Loomis in ...
of
Hazardville, Connecticut Hazardville is a section of the town of Enfield, Connecticut, in Hartford County. It is a census-designated place (CDP) that had a total population of 4,599 as of the 2010 census. History Hazardville originated as an industrial village c ...
, the Oriental Powder Company of Windham, Maine, and the Laflin Powder Company of
Newburgh, New York Newburgh is a city in the U.S. state of New York, within Orange County. With a population of 28,856 as of the 2020 census, it is a principal city of the Poughkeepsie–Newburgh–Middletown metropolitan area. Located north of New York City, a ...
. The
Confederate Powderworks The Confederate Powderworks (a.k.a. the Augusta Powderworks) was a gunpowder factory during the American Civil War, the only permanent structures completed by the Confederate States of America.Bragg, C. L. (2001) "The Augusta powder works: The C ...
of
Augusta, Georgia Augusta ( ), officially Augusta–Richmond County, is a consolidated city-county on the central eastern border of the U.S. state of Georgia. The city lies across the Savannah River from South Carolina at the head of its navigable portion. Geor ...
produced 6,000 tonnes of gunpowder from 1862 to 1865, but was dismantled after the war. The Laflin company merged into the
Laflin & Rand Powder Company Laflin & Rand Powder Company was a gunpowder and early smokeless powder manufacturer notable for producing the smokeless powder used by United States Army infantry rifles from 1896 to 1908, which included the period of development of the M1903 Spri ...
after the war, and with the other three large northern mills formed the United States Gunpowder Trade Association in 1872 including the
American Powder Mills American Powder Mills (1883–1929) was a Massachusetts gunpowder manufacturing complex on the Assabet River. It expanded to include forty buildings along both sides of the river in the towns of Acton, Concord, Maynard, and Sudbury. Press mills, ...
of Maynard, Massachusetts, the
Austin Powder Company Austin Cartridge Company was an Austin Powder Company subsidiary manufacturing cartridge ammunition for small arms. The company made shotgun shells and rimfire cartridges from 1895 until purchased by Western Cartridge Company in 1907. History A ...
of
Glenwillow, Ohio Glenwillow is a village in Cuyahoga County, Ohio, United States. The population was 923 at the 2010 census. History The Village of Glenwillow was carved out of Solon Township and established in 1893 as a company town by Austin Powder Company. A ...
, and the
Miami Powder Company Miami Powder Company operated a gunpowder manufacturing complex on the Little Miami River at Goes Station, Ohio from 1855 to 1925. Willows growing along the banks of the Little Miami River provided the charcoal required for gunpowder. Production ...
of
Goes Station, Ohio Goes Station (also known as Goes) is a small unincorporated community in northern Xenia Township, Greene County, Ohio, United States. It sits at the intersection of Snively Road and U.S. Route 68 between Xenia and Yellow Springs. The communit ...
. Most smaller mills were unable to compete with this trade association, popularly known as the powder trust; although regionally important mills including the California Powder Works of
Santa Cruz, California Santa Cruz ( Spanish for "Holy Cross") is the county seat and largest city of Santa Cruz County, in Northern California. As of the 2020 census, the city population was 62,956. Situated on the northern edge of Monterey Bay, Santa Cruz is a po ...
, the Equitable Powder Company of
East Alton, Illinois East Alton is a village in Madison County, Illinois, United States. The population was 6,301 at the 2010 census. History East Alton was incorporated as a village in 1893 (some say 1894). William Cobb, namesake of Cobb Street, was one of the fir ...
, and the Great Western Powder Works of Kings Mills, Ohio successfully transitioned to manufacture of
smokeless powder Finnish smokeless powderSmokeless powder is a type of propellant used in firearms and artillery that produces less smoke and less fouling when fired compared to gunpowder ("black powder"). The combustion products are mainly gaseous, compared t ...
cartridges. As smokeless powder and
high explosive An explosive (or explosive material) is a reactive substance that contains a great amount of potential energy that can produce an explosion if released suddenly, usually accompanied by the production of light, heat, sound, and pressure. An ...
s replaced gunpowder for most purposes, DuPont became the major manufacturer of United States gunpowder until discontinuing production in 1971. Subsequent production for use in
pyrotechnics Pyrotechnics is the science and craft of creating such things as fireworks, safety matches, oxygen candles, explosive bolts and other fasteners, parts of automotive airbags, as well as gas-pressure blasting in mining, quarrying, and demolition ...
and antique
firearm A firearm is any type of gun designed to be readily carried and used by an individual. The term is legally defined further in different countries (see Legal definitions). The first firearms originated in 10th-century China, when bamboo tubes ...
s has been undertaken by smaller firms whose operations are often ended by the persistent hazard of accidental explosions.


Europe

Notable European mills include: * Ballincollig Royal Gunpowder Mills,
Cork Cork or CORK may refer to: Materials * Cork (material), an impermeable buoyant plant product ** Cork (plug), a cylindrical or conical object used to seal a container ***Wine cork Places Ireland * Cork (city) ** Metropolitan Cork, also known as G ...
,
Ireland Ireland ( ; ga, Éire ; Ulster-Scots: ) is an island in the North Atlantic Ocean, in north-western Europe. It is separated from Great Britain to its east by the North Channel, the Irish Sea, and St George's Channel. Ireland is the s ...
*
Faversham explosives industry Faversham, in Kent, England, has claims to be the cradle of the UK's explosives industry: it was also to become one of its main centres. The first gunpowder plant in the UK was established in the 16th century, possibly at the instigation of the ...
,
Faversham Faversham is a market town in Kent, England, from London and from Canterbury, next to the Swale, a strip of sea separating mainland Kent from the Isle of Sheppey in the Thames Estuary. It is close to the A2, which follows an ancient Briti ...
, England * Grenelle Mill - France * Poudrerie nationale de Vonges, Vonges, Côte-d'Or, France * Waltham Abbey Royal Gunpowder Mills, Waltham Abbey, Essex, England


References

{{Authority control Firearm industry Grinding mills