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A vacuum flask (also known as a Dewar flask, Dewar bottle or thermos) is an insulating storage vessel that greatly lengthens the time over which its contents remain hotter or cooler than the flask's surroundings. Invented by Sir James Dewar in 1892, the vacuum flask consists of two flasks, placed one within the other and joined at the neck. The gap between the two flasks is partially evacuated of air, creating a near-
vacuum A vacuum is a space devoid of matter. The word is derived from the Latin adjective ''vacuus'' for "vacant" or " void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressure. Physicists often di ...
which significantly reduces heat transfer by conduction or
convection Convection is single or multiphase fluid flow that occurs spontaneously due to the combined effects of material property heterogeneity and body forces on a fluid, most commonly density and gravity (see buoyancy). When the cause of the c ...
. When used to hold cold liquids, this also virtually eliminates condensation on the outside of the flask. Vacuum flasks are used domestically to keep
beverage A drink or beverage is a liquid intended for human consumption. In addition to their basic function of satisfying thirst, drinks play important roles in human culture. Common types of drinks include plain drinking water, milk, juice, smoothies ...
s hot or cold for extended periods of time, and for keeping cooked food hot. They are also used for
thermal cooking A thermal cooker, or a vacuum flask cooker, is a cooking device that uses thermal insulation to retain heat and cook food without the continuous use of fuel or other heat source. It is a modern implementation of a haybox, which uses hay or straw ...
. Vacuum flasks are also used for many purposes in industry.


History

The vacuum flask was designed and invented by Scottish scientist Sir James Dewar in 1892 as a result of his research in the field of cryogenics and is sometimes called a Dewar flask in his honour. While performing experiments in determining the specific heat of the element palladium, Dewar made a brass chamber that he enclosed in another chamber to keep the palladium at its desired temperature. He evacuated the air between the two chambers, creating a partial vacuum to keep the temperature of the contents stable. Dewar refused to patent his invention, and the flask, as developed by others using new materials such as
glass Glass is a non-Crystallinity, crystalline, often transparency and translucency, transparent, amorphous solid that has widespread practical, technological, and decorative use in, for example, window panes, tableware, and optics. Glass is most ...
and
aluminium Aluminium (aluminum in AmE, American and CanE, Canadian English) is a chemical element with the Symbol (chemistry), symbol Al and atomic number 13. Aluminium has a density lower than those of other common metals, at approximately o ...
, became a significant tool for chemical experiments and also a common household item. Dewar's design was quickly transformed into a commercial item in 1904 as two German glassblowers, Reinhold Burger and Albert Aschenbrenner, discovered that it could be used to keep cold drinks cold and warm drinks warm and invented a more robust flask design, which was suited for everyday use. The Dewar flask design had never been patented but the German men who discovered the commercial use for the product named it ''Thermos'', and subsequently claimed both the rights to the commercial product and the trademark to the name. In his subsequent attempt to claim the rights to the invention, Dewar instead lost a court case to the company. The manufacturing and performance of the Thermos bottle was significantly improved and refined by the Viennese inventor and merchant Gustav Robert Paalen, who designed various types for domestic use, which he also patented, and distributed widely, through the Thermos Bottle Companies in the United States, Canada and the UK, which bought licences for respective national markets. The American Thermos Bottle Company built up a mass production in Norwich, CT, which brought prices down and enabled the wide distribution of the product for at-home use. Over time, the company expanded the size, shapes and materials of these consumer products, primarily used for carrying
coffee Coffee is a drink prepared from roasted coffee beans. Darkly colored, bitter, and slightly acidic, coffee has a stimulating effect on humans, primarily due to its caffeine content. It is the most popular hot drink in the world. Seeds of ...
on the go and carrying liquids on camping trips to keep them either hot or cold. Eventually other manufacturers produced similar products for consumer use. The name later became a genericized trademark after the term "thermos" became the household name for such a vacuum-insulated container for liquids. The vacuum flask went on to be used for many different types of scientific experiments and the commercial "Thermos" was transformed into a common item. ''Thermos'' remains a registered trademark in some countries, but it was declared a genericized trademark by court action in the United States in 1963, since it had become colloquially synonymous with vacuum flasks in general. However, there are other vacuum flasks.


Design

The vacuum flask consists of two vessels, one placed within the other and joined at the neck. The gap between the two vessels is partially evacuated of air, creating a partial-
vacuum A vacuum is a space devoid of matter. The word is derived from the Latin adjective ''vacuus'' for "vacant" or " void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressure. Physicists often di ...
which reduces heat conduction or
convection Convection is single or multiphase fluid flow that occurs spontaneously due to the combined effects of material property heterogeneity and body forces on a fluid, most commonly density and gravity (see buoyancy). When the cause of the c ...
. Heat transfer by
thermal radiation Thermal radiation is electromagnetic radiation generated by the thermal motion of particles in matter. Thermal radiation is generated when heat from the movement of charges in the material (electrons and protons in common forms of matter) is ...
may be minimized by silvering flask surfaces facing the gap but can become problematic if the flask's contents or surroundings are very hot; hence vacuum flasks usually hold contents below the boiling point of water. Most heat transfer occurs through the neck and opening of the flask, where there is no vacuum. Vacuum flasks are usually made of
metal A metal (from Greek μέταλλον ''métallon'', "mine, quarry, metal") is a material that, when freshly prepared, polished, or fractured, shows a lustrous appearance, and conducts electricity and heat relatively well. Metals are typi ...
, borosilicate glass,
foam Foams are materials formed by trapping pockets of gas in a liquid or solid. A bath sponge and the head on a glass of beer are examples of foams. In most foams, the volume of gas is large, with thin films of liquid or solid separating the ...
or
plastic Plastics are a wide range of synthetic or semi-synthetic materials that use polymers as a main ingredient. Their plasticity makes it possible for plastics to be moulded, extruded or pressed into solid objects of various shapes. This adaptab ...
and have their opening stoppered with cork or polyethylene plastic. Vacuum flasks are often used as insulated shipping containers. Extremely large or long vacuum flasks sometimes cannot fully support the inner flask from the neck alone, so additional support is provided by ''spacers'' between the interior and exterior shell. These spacers act as a thermal bridge and partially reduce the insulating properties of the flask around the area where the spacer contacts the interior surface. Several technological applications, such as NMR and MRI machines, rely on the use of double vacuum flasks. These flasks have two vacuum sections. The inner flask contains liquid
helium Helium (from el, ἥλιος, helios, lit=sun) is a chemical element with the symbol He and atomic number 2. It is a colorless, odorless, tasteless, non-toxic, inert, monatomic gas and the first in the noble gas group in the periodic table. ...
and the outer flask contains liquid nitrogen, with one vacuum section in between. The loss of precious helium is limited in this way. Other improvements to the vacuum flask include the ''vapour-cooled radiation shield'' and the ''vapour-cooled neck'', both of which help to reduce evaporation from the flask.


Research and industry

In laboratories and industry, vacuum flasks are often used to hold liquefied gases (commonly liquid nitrogen with a boiling point of 77 K) for flash freezing, sample preparation and other processes where creating or maintaining an extreme low temperature is desired. Larger vacuum flasks store liquids that become gaseous at well below ambient temperature, such as
oxygen Oxygen is the chemical element with the symbol O and atomic number 8. It is a member of the chalcogen group in the periodic table, a highly reactive nonmetal, and an oxidizing agent that readily forms oxides with most elements as we ...
and
nitrogen Nitrogen is the chemical element with the symbol N and atomic number 7. Nitrogen is a nonmetal and the lightest member of group 15 of the periodic table, often called the pnictogens. It is a common element in the universe, estimated at seve ...
; in this case the leakage of heat into the extremely cold interior of the bottle results in a slow boiling-off of the liquid so that a narrow unstoppered opening, or a stoppered opening protected by a pressure relief valve, is necessary to prevent
pressure Pressure (symbol: ''p'' or ''P'') is the force applied perpendicular to the surface of an object per unit area over which that force is distributed. Gauge pressure (also spelled ''gage'' pressure)The preferred spelling varies by country a ...
from building up and eventually shattering the flask. The insulation of the vacuum flask results in a very slow "boil" and thus the contents remain liquid for long periods without
refrigeration The term refrigeration refers to the process of removing heat from an enclosed space or substance for the purpose of lowering the temperature.International Dictionary of Refrigeration, http://dictionary.iifiir.org/search.phpASHRAE Terminology, ht ...
equipment. Vacuum flasks have been used to house standard cells and ovenized Zener diodes, along with their printed circuit board, in precision voltage-regulating devices used as electrical standards. The flask helped with controlling the Zener temperature over a long time span and was used to reduce variations of the output voltage of the Zener standard owing to temperature fluctuation to within a few parts per million. One notable use was by Guildline Instruments, of Canada, in their Transvolt, model 9154B, saturated standard cell, which is an electrical voltage standard. Here a silvered vacuum flask was encased in foam insulation and, using a large glass vacuum plug, held the saturated cell. The output of the device was 1.018 volts and was held to within a few parts per million. The principle of the vacuum flask makes it ideal for storing certain types of rocket fuel, and
NASA The National Aeronautics and Space Administration (NASA ) is an independent agency of the US federal government responsible for the civil space program, aeronautics research, and space research. NASA was established in 1958, succeedi ...
used it extensively in the propellant tanks of the Saturn launch vehicles in the 1960s and 1970s. The design and shape of the Dewar flask was used as a model for
optical Optics is the branch of physics that studies the behaviour and properties of light, including its interactions with matter and the construction of instruments that use or detect it. Optics usually describes the behaviour of visible, ultrav ...
experiments based on the idea that the shape of the two compartments with the space in between is similar to the way the light hits the eye. The vacuum flask has also been part of experiments using it as the capacitor of different chemicals in order to keep them at a consistent temperature. The industrial Dewar flask is the base for a device used to passively insulate medical shipments. Most vaccines are sensitive to heat and require a cold chain system to keep them at stable, near freezing temperatures. The Arktek device uses eight one-litre ice blocks to hold vaccines at under 10
°C The degree Celsius is the unit of temperature on the Celsius scale (originally known as the centigrade scale outside Sweden), one of two temperature scales used in the International System of Units (SI), the other being the Kelvin scale. The d ...
. In the oil and gas industry, Dewar flasks are used to insulate the electronic components in wireline logging tools. Conventional logging tools (rated to 350°F) are upgraded to high-temperature specifications by installing all sensitive electronic components in a Dewar flask. Baird, Tom, et al. "High-pressure, high-temperature well logging, perforating and testing." ''Oilfield Review'' 5.2/3 (1993): 15-32.


Safety

Vacuum flasks are at risk of implosion hazard, and glass vessels under vacuum, in particular, may shatter unexpectedly. Chips, scratches or cracks can be a starting point for dangerous vessel failure, especially when the vessel temperature changes rapidly (when hot or cold liquid is added). Proper preparation of the Dewar vacuum flask by tempering prior to use is advised to maintain and optimize the functioning of the unit. Glass vacuum flasks are usually fitted into a metal base with the cylinder contained in or coated with mesh, aluminum or plastic to aid in handling, protect it from physical damage, and contain fragments should they break. In addition, cryogenic storage dewars are usually pressurized, and they may explode if pressure relief valves are not used. Thermal expansion has to be taken into account when engineering a vacuum flask. The outer and inner walls are exposed to different temperatures and will expand at different rates. The vacuum flask can rupture due to the differential in thermal expansion between the outer and inner walls. Expansion joints are commonly used in tubular vacuum flasks to avoid rupture and maintain vacuum integrity.


See also

*
Thermal cooking A thermal cooker, or a vacuum flask cooker, is a cooking device that uses thermal insulation to retain heat and cook food without the continuous use of fuel or other heat source. It is a modern implementation of a haybox, which uses hay or straw ...
* Hermetic seal *
Sunshield (JWST) The James Webb Space Telescope (JWST) sunshield is a passive thermal control system deployed post-launch to shield the telescope and instrumentation from the light and heat of the Sun, Earth, and Moon. By keeping the telescope and instrumen ...
(The layers of its thermal shield use a vacuum barrier to provide insulation.) * Tervis Tumbler * Yeti Holdings


References


Further reading

* Burger, R., , ''"Double walled vessel with a space for a vacuum between the walls,"'' December 3, 1907. *


External links

* {{Authority control 1892 introductions Cryogenics Scottish inventions 19th-century inventions Containers