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Striations are marks produced on the fracture surface that show the incremental growth of a
fatigue Fatigue describes a state of tiredness that does not resolve with rest or sleep. In general usage, fatigue is synonymous with extreme tiredness or exhaustion that normally follows prolonged physical or mental activity. When it does not resolve ...
crack. A striation marks the position of the crack tip at the time it was made. The term ''striation'' generally refers to ''ductile striations'' which are rounded bands on the fracture surface separated by depressions or fissures and can have the same appearance on both sides of the mating surfaces of the fatigue crack. Although some research has suggested that many loading cycles are required to form a single striation, it is now generally thought that each striation is the result of a single loading cycle. The presence of striations is used in
failure analysis Failure analysis is the process of collecting and analyzing data to determine the cause of a failure, often with the goal of determining corrective actions or liability. According to Bloch and Geitner, ”machinery failures reveal a reaction chain o ...
as an indication that a fatigue crack has been growing. Striations are generally not seen when a crack is small even though it is growing by fatigue, but will begin to appear as the crack becomes larger. Not all periodic marks on the fracture surface are striations. The size of a striation for a particular material is typically related to the magnitude of the loading characterised by
stress intensity factor In fracture mechanics, the stress intensity factor () is used to predict the stress state ("stress intensity") near the tip of a crack or notch caused by a remote load or residual stresses. It is a theoretical construct usually applied to a h ...
range, the mean stress and the environment. The width of a striation is indicative of the overall crack growth rate but can be locally faster or slower on the fracture surface.


Striation features

The study of the fracture surface is known as
fractography Fractography is the study of the fracture surfaces of materials. Fractographic methods are routinely used to determine the cause of failure in engineering structures, especially in product failure and the practice of forensic engineering or fa ...
. Images of the crack can be used to reveal features and understand the mechanisms of crack growth. While striations are fairly straight, they tend to curve at the ends allowing the direction of crack growth to be determined from an image. Striations generally form at different levels in metals and are separated by a ''tear band'' between them. Tear bands are approximately parallel to the direction of crack growth and produce what is known as a ''river pattern'', so called, because it looks like the diverging pattern seen with river flows. The source of the river pattern converges to a single point that is typically the origin of the fatigue failure. Striations can appear on both sides of the mating fracture surface. There is some dispute as to whether striations produced on both sides of the fracture surface match peak-to-peak or peak-to-valley. The shape of striations may also be different on each side of the fracture surface. Striations do not occur uniformly over all of the fracture surface and many areas of a fatigue crack may be devoid of striations. Striations are most often observed in metals but also occur in plastics such as
Poly(methyl_methacrylate) Poly(methyl methacrylate) (PMMA) belongs to a group of materials called engineering plastics. It is a transparent thermoplastic. PMMA is also known as acrylic, acrylic glass, as well as by the trade names and brands Crylux, Plexiglas, Acrylite, ...
. Small striations can be seen with the aid of a scanning electron microscope. Once the size of a striation is over 500 nm (resolving wavelength of light), they can be seen with an
optical microscope The optical microscope, also referred to as a light microscope, is a type of microscope that commonly uses visible light and a system of lenses to generate magnified images of small objects. Optical microscopes are the oldest design of microsco ...
. The first image of striations was taken by Zapffe and Worden in 1951 using an optical microscope. The width of a striation indicates the local rate of crack growth and is typical of the overall rate of growth over the fracture surface. The rate of growth can be predicted with a
crack growth equation A crack growth equation is used for calculating the size of a fatigue crack growing from cyclic loads. The growth of fatigue cracks can result in catastrophic failure, particularly in the case of aircraft. A crack growth equation can be used to en ...
such as the Paris-Erdogan equation. Defects such as inclusions and grain boundaries may locally slow down the rate of growth. ''Variable amplitude'' loads produce striations of different widths and the study of these striation patterns has been used to understand fatigue. Although various cycle counting methods can be used to extract the equivalent constant amplitude cycles from a variable amplitude sequence, the striation pattern differs from the cycles extracted using the rainflow counting method. The height of a striation has been related to the ''stress ratio'' R of the applied loading cycle, where R = K_\text/K_\text and is thus a function of the minimum K_\text and maximum K_\text stress intensity of the applied loading cycle. The striation profile depends on the degree of loading and unloading in each cycle. The unloading part of the cycle causing plastic deformation on the surface of the striation. Crack extension only occurs from the rising part of the load cycle.


Striation-like features

Other periodic marks on the fracture surface can be mistaken for striations.


Marker bands

Variable amplitude loading causes cracks to change the plane of growth and this effect can be used to create ''marker bands'' on the fracture surface. When a number of constant amplitude cycles are applied they may produce a plateau of growth on the fracture surface. Marker bands (also known as ''progression marks'' or ''beach marks'') may be produced and readily identified on the fracture surface even though the magnitude of the loads may too small to produce individual striations. In addition, marker bands may also be produced by large loads (also known as overloads) producing a region of ''fast fracture'' on the crack surface. Fast fracture can produce a region of rapid extension before blunting of the crack tip stops the growth and further growth occurs during fatigue. Fast fracture occurs through a process of
microvoid coalescence Microvoid coalescence (MVC) is a high energy microscopic fracture mechanism observed in the majority of metallic alloys and in some engineering plastics. Fracture process MVC proceeds in three stages: nucleation, growth, and coalescence of m ...
where failures initiate around inter-metallic particles. The F111 aircraft was subjected to periodic proof testing to ensure any cracks present were smaller than a certain critical size. These loads left marks on the fracture surface that could be identified, allowing the rate of intermediate growth occurring in service to be measured. Marks also occur from a change in the environment where oil or corrosive environments can deposit or from excessive heat exposure and colour the fracture surface up to the current position of the crack tip. Marker bands may be used to measure the instantaneous rate of growth of the applied loading cycles. By applying a repeated sequence separated by loads that produce a distinctive pattern the growth from each segment of loading can be measured using a microscope in a technique called ''quantitative fractography'', the rate of growth for loading segments of ''constant amplitude'' or ''variable amplitude'' loading can be directly measured from the fracture surface.


Tyre tracks

''Tyre tracks'' are the marks on the fracture surface produced by something making an impression onto the surface from the repeated opening and closing of the crack faces. This can be produced by either a particle that becomes trapped between the crack faces or the faces themselves shifting and directly contacting the opposite surface.


Coarse striations

''Coarse striations'' are a general rumpling of the fracture surface and do not correspond to a single loading cycle and are therefore not considered to be true striations. They are produced instead of regular striations when there is insufficient atmospheric moisture to form hydrogen on the surface of the crack tip in aluminium alloys, thereby preventing the slip planes activation. The wrinkles in the surface cross over and so do not represent the position of the crack tip.


Striation formation in aluminium


Environmental influence

Striations are often produced in high strength aluminium alloys. In these alloys, the presence of ''water vapour'' is necessary to produce ductile striations, although too much water vapour will produce ''brittle striations'' also known as ''cleavage striations''. Brittle striations are flatter and larger than ductile striations produced with the same load. There is sufficient water vapour present in the atmosphere to generate ductile striations. Cracks growing internally are isolated from the atmosphere and grow in a
vacuum A vacuum is a space devoid of matter. The word is derived from the Latin adjective ''vacuus'' for "vacant" or "void". An approximation to such vacuum is a region with a gaseous pressure much less than atmospheric pressure. Physicists often dis ...
. When water vapour deposits onto the freshly exposed aluminium fracture surface, it dissociates into
hydroxides Hydroxide is a polyatomic ion, diatomic anion with chemical formula OH−. It consists of an oxygen and hydrogen atom held together by a single covalent bond, and carries a negative electric charge. It is an important but usually Self-ionization ...
and atomic
hydrogen Hydrogen is the chemical element with the symbol H and atomic number 1. Hydrogen is the lightest element. At standard conditions hydrogen is a gas of diatomic molecules having the formula . It is colorless, odorless, tasteless, non-toxic, an ...
. Hydrogen interacts with the crack tip affecting the appearance and size of the striations. The growth rate increases typically by an order of magnitude, with the presence of water vapour. The mechanism is thought to be
hydrogen embrittlement Hydrogen embrittlement (HE), also known as hydrogen-assisted cracking or hydrogen-induced cracking (HIC), is a reduction in the ductility of a metal due to absorbed hydrogen. Hydrogen atoms are small and can permeate solid metals. Once absorbed ...
as a result of hydrogen being absorbed into the plastic zone at the crack tip. When an internal crack breaks through to the surface, the rate of crack growth and the fracture surface appearance will change due to the presence of water vapour. Coarse striations occur when a fatigue crack grows in a vacuum such as when growing from an internal flaw.


Cracking plane

In aluminium (a
face-centred cubic In crystallography, the cubic (or isometric) crystal system is a crystal system where the unit cell is in the shape of a cube. This is one of the most common and simplest shapes found in crystals and minerals. There are three main varieties of ...
material), cracks grow close to low index planes such as the and the planes (see
Miller Index Miller indices form a notation system in crystallography for lattice planes in crystal (Bravais) lattices. In particular, a family of lattice planes of a given (direct) Bravais lattice is determined by three integers ''h'', ''k'', and '' ...
). Both of these planes bisect a pair of slip planes. Crack growth involving a single slip plane is term ''Stage I'' growth and crack growth involving two slip planes is termed ''Stage II'' growth. Striations are typically only observed in Stage II growth. Brittle striations are typically formed on planes.


Models of striation formation

There have been many models developed to explain the process of how a striation is formed and their resultant shape. Some of the significant models are: * Plastic blunting model of Laird * Saw-tooth model of McMillan and Pelloux * Coarse slip model of Neumman * Shear band model by Zhang


References

{{Reflist


External links


Characteristics of a fatigue failure in metals
Materials science Reliability engineering Fracture mechanics Materials degradation Mechanical failure modes