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Nuclear densitometry is a technique used in civil construction and the
petroleum industry
The petroleum industry, also known as the oil industry or the oil patch, includes the global processes of exploration, extraction, refining, transportation (often by oil tankers and pipelines), and marketing of petroleum products. The larges ...
, as well as for mining and archaeology purposes, to measure the density and inner structure of the test material. The processes uses a nuclear density gauge, which consists of a
radiation
In physics, radiation is the emission or transmission of energy in the form of waves or particles through space or through a material medium. This includes:
* ''electromagnetic radiation'', such as radio waves, microwaves, infrared, visi ...
source that emits particles and a
sensor
A sensor is a device that produces an output signal for the purpose of sensing a physical phenomenon.
In the broadest definition, a sensor is a device, module, machine, or subsystem that detects events or changes in its environment and sends ...
that counts the received particles that are either reflected by the test material or pass through it. By calculating the percentage of particles that return to the sensor, the gauge can be calibrated to measure the density.
In
geotechnical engineering
Geotechnical engineering is the branch of civil engineering concerned with the engineering behavior of earth materials. It uses the principles of soil mechanics and rock mechanics for the solution of its respective engineering problems. It als ...
, a nuclear densometer or ''soil density gauge'' is a field instrument used to determine the density of a compacted material. The device uses the interaction of
gamma radiation
A gamma ray, also known as gamma radiation (symbol γ or \gamma), is a penetrating form of electromagnetic radiation arising from the radioactive decay of atomic nuclei. It consists of the shortest wavelength electromagnetic waves, typically s ...
with matter to measure density, either through direct transmission or the "backscatter" method. The device determines the density of material by counting the number of photons emitted by a radioactive source (cesium-137) that are read by the detector tubes in the gauge base. A 60-second time interval is typically used for the counting period.
Sources
Different variants are used for different purposes. For density analysis of very shallow objects such as roads or walls, a
gamma
Gamma (uppercase , lowercase ; ''gámma'') is the third letter of the Greek alphabet. In the system of Greek numerals it has a value of 3. In Ancient Greek, the letter gamma represented a voiced velar stop . In Modern Greek, this letter re ...
source emitter such as
137Cesium
Caesium (IUPAC spelling) (or cesium in American English) is a chemical element with the symbol Cs and atomic number 55. It is a soft, silvery-golden alkali metal with a melting point of , which makes it one of only five elemental metals that ar ...
is used to produce gamma radiation. These isotopes are effective in analyzing the top 10 inches (25 centimeters) with high accuracy.
226Radium
Radium is a chemical element with the symbol Ra and atomic number 88. It is the sixth element in group 2 of the periodic table, also known as the alkaline earth metals. Pure radium is silvery-white, but it readily reacts with nitrogen (rather t ...
is used for depths of 328 yards (300 meters). Such instruments can help find caves or identify locations with lower density that would make tunnel construction hazardous.
Modes of use
Nuclear density gauges are typically operated in one of two modes:
Direct transmission: The retractable rod is lowered into the mat through a pre-drilled hole. The source emits radiation, which then interact with
electrons
The electron ( or ) is a subatomic particle with a negative one elementary electric charge. Electrons belong to the first generation of the lepton particle family,
and are generally thought to be elementary particles because they have no ...
in the material and lose energy and/or are redirected (
scattered
Scattered may refer to:
Music
* ''Scattered'' (album), a 2010 album by The Handsome Family
* "Scattered" (The Kinks song), 1993
* "Scattered", a song by Ace Young
* "Scattered", a song by Lauren Jauregui
* "Scattered", a song by Green Day from ' ...
). Radiation that loses sufficient energy or is scattered away from the detector is not counted. The denser the material, the higher the probability of interaction and the lower the detector count. Therefore, the detector count is inversely proportional to material density. A calibration factor is used to relate the count to the actual density.
Backscatter: The retractable rod is lowered so that it is even with the detector but still within the instrument. The source emits radiation, which then interact with electrons in the material and lose energy and/or are redirected (scattered). Radiation that is scattered towards the detector is counted. The denser the material, the higher the probability that radiation will be redirected towards the detector. Therefore, the detector count is proportional to the density. A calibration factor is used to correlate the count to the actual density.
Many devices are built to measure both the density and
moisture content
Water content or moisture content is the quantity of water contained in a material, such as soil (called soil moisture), rock, ceramics, crops, or wood. Water content is used in a wide range of scientific and technical areas, and is expressed as a ...
of material. This is important to the
civil construction
Construction is a general term meaning the art and science to form objects, systems, or organizations,"Construction" def. 1.a. 1.b. and 1.c. ''Oxford English Dictionary'' Second Edition on CD-ROM (v. 4.0) Oxford University Press 2009 and com ...
industry specifically as both are essential to verifying suitable soil conditions to support structures, streets, highways, and airport runways.
Uses
Ground compaction
![Density Meter Asphalt](https://upload.wikimedia.org/wikipedia/commons/4/4e/Density_Meter_Asphalt.jpg)
A nuclear densometer is used on a compacted base to establish its percentage of compaction.
Before field tests are performed, the technician performs a calibration on the gauge which records the 'standard count' of the machine. Standard counts are the amount of radiation released by the two nuclear sources inside the machine, with no loss or leakage. This allows the machine to compare the amount of radiation released to the amount of radiation received. With the use of a 3/4" diameter rod a hole is created in the compacted base by hammering the rod into the base to produce a hole that the densometer's probe can be inserted into. The densometer is placed on top of the hole, and then the probe is inserted into the hole by unlocking the handle at the top of the probe. One source produces radiation that interacts with the atoms in the soil, and is then compared to the standard count, to calculate the density. The other source interacts with
hydrogen
Hydrogen is the chemical element with the symbol H and atomic number 1. Hydrogen is the lightest element. At standard conditions hydrogen is a gas of diatomic molecules having the formula . It is colorless, odorless, tasteless, non-toxic, an ...
atoms to calculate the percentage of water in the soil.
In direct transmission mode, the source extends through the base of the gauge into a predrilled hole, positioning the source at the desired depth. The testing procedure is analogous to burying a known quantity of radioactive material at a specific depth, and then using a
Geiger counter
A Geiger counter (also known as a Geiger–Müller counter) is an electronic instrument used for detecting and measuring ionizing radiation. It is widely used in applications such as radiation dosimetry, radiological protection, experimental ph ...
at the ground surface to measure how effectively the soil's density blocks the penetration of gamma radiation through the soil. As the soil's density increases, less radiation can pass through it, owing to dispersion from collisions with electrons in the soil being tested.
Since the soil's moisture level is partly responsible for its in-place density, the gauge also contains a
neutron moisture gauge
A neutron moisture meter is a moisture meter utilizing neutron scattering. The meters are most frequently used to measure the water content in soil or rock. The technique is non-destructive, and is sensitive to moisture in the bulk of the target m ...
consisting of an
americium
Americium is a synthetic radioactive chemical element with the symbol Am and atomic number 95. It is a transuranic member of the actinide series, in the periodic table located under the lanthanide element europium, and thus by analogy was na ...
/
beryllium
Beryllium is a chemical element with the symbol Be and atomic number 4. It is a steel-gray, strong, lightweight and brittle alkaline earth metal. It is a divalent element that occurs naturally only in combination with other elements to form mi ...
high-energy
neutron source
A neutron source is any device that emits neutrons, irrespective of the mechanism used to produce the neutrons. Neutron sources are used in physics, engineering, medicine, nuclear weapons, petroleum exploration, biology, chemistry, and nuclear p ...
and a
thermal neutron
The neutron detection temperature, also called the neutron energy, indicates a free neutron's kinetic energy, usually given in electron volts. The term ''temperature'' is used, since hot, thermal and cold neutrons are moderated in a medium with ...
detector. The high-energy neutrons are slowed when they collide with hydrogen atoms, and the detector then counts the "slowed" neutrons. This count is proportional to the soil's water content, since the hydrogen in this water (H
2O) is responsible for almost all the hydrogen found in most soils. The gauge calculates the moisture content, subtracts it from the soil's in-place (wet) density, and reports the soil's dry density.
Density of liquids in pipes
Nuclear density gauges can also be used to measure the density of a liquid in a pipe. If a source is mounted on one side of a pipe and a detector on the other, the amount of radiation seen at the detector is dependent upon the shielding provided by the liquid in the pipe.
Tracerco
Tracerco is the oil and gas services subsidiary of British chemical company and conglomerate Johnson Matthey.
History
In 1958, Imperial Chemical Industries ( ICI) established a division to research the use of ionizing radiation within chemical ...
pioneered the use of radiation to measure density in the 1950s and determined that the
Beer–Lambert law
The Beer–Lambert law, also known as Beer's law, the Lambert–Beer law, or the Beer–Lambert–Bouguer law relates the attenuation of light to the properties of the material through which the light is travelling. The law is commonly applied t ...
also applied to radiation as well as optics. Gauges are normally calibrated using gas and a liquid of known density to find the unknowns in the equation. Once it has been calibrated and as long as the source detector alignment remains constant, it is possible to calculate the density of the liquid in the pipe. One factor is the
half-life
Half-life (symbol ) is the time required for a quantity (of substance) to reduce to half of its initial value. The term is commonly used in nuclear physics to describe how quickly unstable atoms undergo radioactive decay or how long stable ato ...
of the radioactive source (30 years for
137Cs), which means that the system needs to be recalibrated at regular intervals. Modern systems incorporate correction for source decay.
Locating underground water
Another variant is to use a strong neutron source like
241americium/beryllium to produce
neutron radiation
Neutron radiation is a form of ionizing radiation that presents as free neutrons. Typical phenomena are nuclear fission or nuclear fusion causing the release of free neutrons, which then Neutron capture, react with Atomic nucleus, nuclei of other ...
and then measure the energy of returning
neutron scattering
Neutron scattering, the irregular dispersal of free neutrons by matter, can refer to either the naturally occurring physical process itself or to the man-made experimental techniques that use the natural process for investigating materials. Th ...
. As
hydrogen
Hydrogen is the chemical element with the symbol H and atomic number 1. Hydrogen is the lightest element. At standard conditions hydrogen is a gas of diatomic molecules having the formula . It is colorless, odorless, tasteless, non-toxic, an ...
characteristically slows down neutrons, the sensor can calculate the density of hydrogen - and find pockets of underground water, humidity up to a depth of several meters, moisture content, or asphalt content.
Testing separators
Neutron sources can also be used to assess the performance of a
separator (oil production)
The term separator in oilfield terminology designates a pressure vessel used for separating well fluids produced from oil and gas wells into gaseous and liquid components. A separator for petroleum production is a large vessel designed to separate ...
in the same way. Gas, oil, water and sand all have different concentrations of hydrogen atoms which reflect different amounts of slow neutrons. Using a head which contains an
241AmBe neutron source and a slow
neutron detector
Neutron detection is the effective detection of neutrons entering a well-positioned detector. There are two key aspects to effective neutron detection: hardware and software. Detection hardware refers to the kind of neutron detector used (the most ...
, by scanning it up and down a separator it is possible to determine the interface levels within the separator.
See also
*
Nuclear power
Nuclear power is the use of nuclear reactions to produce electricity. Nuclear power can be obtained from nuclear fission, nuclear decay and nuclear fusion reactions. Presently, the vast majority of electricity from nuclear power is produced b ...
References
{{Geotechnical engineering
Radiography
Density meters
In situ geotechnical investigations