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A loop-gap resonator (LGR) is an electromagnetic resonator that operates in the radio and microwave frequency ranges. The simplest LGRs are made from a conducting tube with a narrow slit cut along its length. The LGR dimensions are typically much smaller than the free-space wavelength of the
electromagnetic field An electromagnetic field (also EM field or EMF) is a classical (i.e. non-quantum) field produced by (stationary or moving) electric charges. It is the field described by classical electrodynamics (a classical field theory) and is the classical c ...
s at the resonant frequency. Therefore, relatively compact LGRs can be designed to operate at frequencies that are too low to be accessed using, for example, cavity resonators. These structures can have very sharp resonances (high
quality factor In physics and engineering, the quality factor or ''Q'' factor is a dimensionless parameter that describes how underdamped an oscillator or resonator is. It is defined as the ratio of the initial energy stored in the resonator to the energy los ...
s) making them useful for
electron spin resonance Electron paramagnetic resonance (EPR) or electron spin resonance (ESR) spectroscopy is a method for studying materials that have unpaired electrons. The basic concepts of EPR are analogous to those of nuclear magnetic resonance (NMR), but the spi ...
(ESR) experiments, and precision measurements of electromagnetic material properties (
permittivity In electromagnetism, the absolute permittivity, often simply called permittivity and denoted by the Greek letter ''ε'' ( epsilon), is a measure of the electric polarizability of a dielectric. A material with high permittivity polarizes more in ...
and permeability).


Background

Loop-gap resonators (LGRs) can be modelled as lumped-element circuits. The slit along the length of the resonator has an effective
capacitance Capacitance is the capability of a material object or device to store electric charge. It is measured by the change in charge in response to a difference in electric potential, expressed as the ratio of those quantities. Commonly recognized are ...
C and the bore of the resonator has effective
inductance Inductance is the tendency of an electrical conductor to oppose a change in the electric current flowing through it. The flow of electric current creates a magnetic field around the conductor. The field strength depends on the magnitude of the ...
L. At, or near, the resonance frequency, a circumferential current is established along the inner wall of the resonator. The effective resistance R that limits this current is, in part, determined by the
resistivity Electrical resistivity (also called specific electrical resistance or volume resistivity) is a fundamental property of a material that measures how strongly it resists electric current. A low resistivity indicates a material that readily allows ...
\rho and electromagnetic skin depth \delta of the conductor used to make the LGR. It is, therefore, possible to model the LGR as an LRC circuit. Since the LGR current is a maximum at the resonant frequency, the equivalent circuit model is a series LRC circuit. This circuit model works well provided the dimensions of the resonator remain small compared to the free-space wavelength of the electromagnetic fields. One advantage of the LGR is that it produces regions of uniform electric and magnetic fields that are isolated from one another. A uniform electric field exists within the slit of the LGR and a uniform magnetic field exists within the bore of the resonator. The uniform magnetic field makes the LGR a good source of microwave magnetic fields in ESR experiments. Furthermore, because the electric and magnetic fields are isolated from one another, one can use the LGR to independently probe the electric and magnetic properties of materials. For example, if the gap of the LGR is filled with a
dielectric In electromagnetism, a dielectric (or dielectric medium) is an electrical insulator that can be polarised by an applied electric field. When a dielectric material is placed in an electric field, electric charges do not flow through the mate ...
material, the effective capacitance of the LGR will be modified which will change the frequency f_0 and quality factor Q of the resonance. Measurements of the changes in f_0 and Q can be used to fully determine the complex permittivity of the dielectric material. Likewise, if the bore of the LGR is filled with a magnetic material, the effective inductance of the LGR will be modified and the resulting changes in f_0 and Q can be used to extract the complex permeability of the magnetic material.


Resonant Frequency and Quality Factor


Resonance frequency

The capacitance of the gap of the LGR is given by : C = \varepsilon_0 \frac \,, where \varepsilon_0 is the
permittivity of free space Vacuum permittivity, commonly denoted (pronounced "epsilon nought" or "epsilon zero"), is the value of the absolute dielectric permittivity of classical vacuum. It may also be referred to as the permittivity of free space, the electric consta ...
, w is the thickness of the bore wall, t is the gap width, and \ell is the length of the resonator. The resonator bore acts as a single-turn
solenoid upright=1.20, An illustration of a solenoid upright=1.20, Magnetic field created by a seven-loop solenoid (cross-sectional view) described using field lines A solenoid () is a type of electromagnet formed by a helix, helical coil of wire whose ...
with inductance given by : L = \mu_0 \frac \,, where \mu_0 is the
permeability of free space The vacuum magnetic permeability (variously ''vacuum permeability'', ''permeability of free space'', ''permeability of vacuum''), also known as the magnetic constant, is the magnetic permeability in a classical vacuum. It is a physical constan ...
and r_0 is the inner radius of the LGR bore. For a high-Q resonator, the resonant frequency is, to an approximation, given by : f_0 \approx \frac\frac=\frac\sqrt\,, where c=1/\sqrt is the
vacuum speed of light The speed of light in vacuum, commonly denoted , is a universal physical constant that is important in many areas of physics. The speed of light is exactly equal to ). According to the special theory of relativity, is the upper limit for ...
. Therefore, the resonant frequency of the LGR is determined from its geometry and is, to first approximation, independent of its length.


Quality factor

For a highly
underdamped Damping is an influence within or upon an oscillatory system that has the effect of reducing or preventing its oscillation. In physical systems, damping is produced by processes that dissipate the energy stored in the oscillation. Examples incl ...
series LRC circuit, the quality factor, which determines the sharpness of the resonance, is given by : Q \approx \frac\sqrt\,. The effective resistance of a LGR can be estimated by considering the length of conductor through which the current travels and the cross-sectional area available to it. The relevant conductor length is the circumference 2\pi r_0 of the conductor's inner surface. The depth that the current penetrates into the inner surface of the LGR bore is determined by the electromagnetic skin depth \delta. Therefore, the cross-sectional area through which charge flows is \delta\,\ell. Combining these results gives an effective resistance : R_\rho \approx \rho\frac\,, where \rho is the resistivity of the conductor. The effective capacitance, inductance, and resistance then lead to a simple expression for the expected quality factor of the LGR : Q \approx \frac\,, where, for a good conductor, the electromagnetic skin depth at the resonance frequency is given by : \delta \approx \sqrt\,, and \omega_0=2\pi f_0. For an aluminum resonator with r_0 =1\,\mathrm and f_0=1\,\mathrm the above analysis predicts Q\approx 3900.


Radiative losses

In practice, the measured quality factor a cylindrical LGR, without additional electromagnetic shielding, will be much less than the predicted value of r_0/\delta. The suppression of the quality factor is due to radiative power loss from magnetic field lines that extend out of LGR bore and into free space. An order-of-magnitude estimate of the effective
radiation resistance Radiation resistance, \ R_\mathsf\ or \ R_\mathsf\ , is proportional to the part of an antenna's feedpoint electrical resistance that is caused by power loss from the emission of radio waves from the antenna. Radiation resistance is an ''effecti ...
can be made by treating the LGR as a conducting loop. In the limit that the wavelength of the radiation is much larger than the loop radius r_0, the radiation resistance is : R_\mathrm \approx \frac\sqrt\left(\frac\right)^4\,, and can be much larger than the resistance R_\rho due to the resistivity of the LGR conductor. The radiative losses can be suppressed by placing the LGR inside a circular
waveguide A waveguide is a structure that guides waves, such as electromagnetic waves or sound, with minimal loss of energy by restricting the transmission of energy to one direction. Without the physical constraint of a waveguide, wave intensities de ...
. Provided that the cutoff frequency of the lowest TE11 waveguide mode is well above the resonant frequency of the LGR, the magnetic field lines will be prevented from propagating into free space. The presence of the electromagnetic shield will alter the resonant frequency and quality factor of the LGR, but typically by only a few percent.


Toroidal LGR

In some applications requiring high quality factors, the electromagnetic shielding provided by a concentric circular waveguide surrounding a cylindrical LGR can be bulky and awkward to work. A toroidal LGR can be used for high-Q measurements without requiring additional electromagnetic shielding. In the toroidal geometry the two ends of a cylindrical LGR are joined to form a completely closed structure. In this case, the magnetic field is completely confined within the bore of the resonator and there is no radiative power loss. The toroidal LGR consists of two halves that are bolted together along the outer diameter of the structure. Like the cylindrical LGR, the toroidal LGR can be modelled as a series LRC circuit. In general, the effective capacitance, inductance, and resistance of the toroidal LGR will differ from the expressions given above for the cylindrical LGR. However, in limit that the radius of the torus is large compared to the bore radius r_0, the capacitance, inductance, and resistance of the toroidal LGR are approximated by the expressions above if one takes \ell to be equal to the circumference of the torus. The toroidal LGR is particularly convenient when characterizing the electromagnetic properties of liquid samples or particles suspended in a liquid. In these cases, the bore of the toroidal LGR can be partially filled with the liquid sample without requiring a special sample holder. This setup allows one to characterize the magnetic properties of, for example, a
ferrofluid Ferrofluid is a liquid that is attracted to the poles of a magnet. It is a colloidal liquid made of nanoscale ferromagnetic or ferrimagnetic particles suspended in a carrier fluid (usually an organic solvent or water). Each magnetic particle ...
. Alternatively, if the liquid sample is nonmagnetic, the entire toroidal LGR can be submerged in the liquid (or gas). In this case, the dielectric properties of the sample only modify the effective capacitance of the resonator and the changes in f_0 and Q can be used to determine the complex permittivity of the sample.


Coupling to a LGR

Inductive coupling In electrical engineering, two conductors are said to be inductively coupled or magnetically coupled when they are configured in a way such that change in current through one wire induces a voltage across the ends of the other wire through el ...
loops are typically used to couple
magnetic flux In physics, specifically electromagnetism, the magnetic flux through a surface is the surface integral of the normal component of the magnetic field B over that surface. It is usually denoted or . The SI unit of magnetic flux is the weber ( ...
into and out of the LGR. The coupling loops are made by first removing a length of outer conductor and dielectric from a semi-rigid
coaxial cable Coaxial cable, or coax (pronounced ) is a type of electrical cable consisting of an inner conductor surrounded by a concentric conducting shield, with the two separated by a dielectric ( insulating material); many coaxial cables also have a p ...
. The exposed centre conductor is then bent into a loop and short-circuited to the outer conductor. The opposite end of the coaxial cable is connected to either a
signal generator A signal generator is one of a class of electronic devices that generates electrical signals with set properties of amplitude, frequency, and wave shape. These generated signals are used as a stimulus for electronic measurements, typically used i ...
or a receiver. In the case of a signal generator, an oscillating current is established in the coupling loop. By
Faraday's law of induction Faraday's law of induction (briefly, Faraday's law) is a basic law of electromagnetism predicting how a magnetic field will interact with an electric circuit to produce an electromotive force (emf)—a phenomenon known as electromagnetic inducti ...
, this current creates and oscillating magnetic flux which can be coupled into the bore of the LGR. This magnetic flux, in turn, induces circumferential currents along the inner wall of the LGR. The induced current, once again by Faraday's law, creates an approximately uniform oscillating magnetic field in the bore of the LGR. A second coupling loop, connected to a receiver, can be used to detect the magnetic flux produced by the LGR. Alternatively, using a
vector network analyzer A network analyzer is an instrument that measures the network parameters of electrical networks. Today, network analyzers commonly measure s–parameters because reflection and transmission of electrical networks are easy to measure at high ...
(VNA), a single coupling loop can be used to both inject a signal into the LGR and measure its response. The VNA can measure the ratio of the forward and reflected voltages (S_, or
reflection coefficient In physics and electrical engineering the reflection coefficient is a parameter that describes how much of a wave is reflected by an impedance discontinuity in the transmission medium. It is equal to the ratio of the amplitude of the reflected wa ...
) as a function of microwave frequency. Far away from resonance, the magnitude of the reflection coefficient will be close to one since very little power is coupled into the LGR at these frequencies. However, near the resonance frequency f_0, the magnitude of the reflection coefficient will fall below one as power is transferred into the LGR. The coupling between the external circuits and the LGR can be tuned by adjusting the relative positions and orientations of the coupling loop and LGR. At critical coupling,
impedance matching In electronics, impedance matching is the practice of designing or adjusting the input impedance or output impedance of an electrical device for a desired value. Often, the desired value is selected to maximize power transfer or minimize signal ...
is achieved and the reflection coefficient approaches zero. It is also possible to capacitively couple electric fields into and out of the gap of the LGR using suitably-fashioned electrodes at the end of a coaxial cable.


Multi-Loop, Multi-Gap LGRs

Multi-loop, multi-gap LGRs have also been developed. The simplest of these is the two-loop, one-gap LGR. In this case, magnetic field lines form closed loops by passing through each of the bores of the LGR and the currents on the inner walls propagate in opposite directions - clockwise in one bore and counterclockwise in the other. The equivalent circuit, neglecting losses, is a parallel combination of inductors L and L_0 in series with capacitance C. If L=L_0, then the resonant frequency of the two-loop, one-gap LGR is \sqrt times greater than that of the conventional one-loop, one-gap LGR having the same bore and gap dimensions. It is also worth noting that, since magnetic field lines pass from one bore to the other, radiative power losses are strongly suppressed and the resonator maintains a high quality factor without requiring additional electromagnetic shielding. The multi-loop, multi-gap LGRs with more than two loops have more than one resonant mode. If the central bore is singled out as having inductance L_0, then one of the resonant modes is one in which all of the magnetic flux from each of the external loops of inductance L is shared with the central loop. For this mode, the resonant frequency of an n-loop, (n-1)-gap LGR is given by : f_0 \approx \frac\sqrt\,, where it has been assumed that all loops have the same inductance L.


LGRs and superconductivity

Loop-gap resonators have been used to make precise measurements of the electrodynamic properties of
unconventional superconductors Unconventional superconductors are materials that display superconductivity which does not conform to either the conventional BCS theory or Nikolay Bogolyubov's theory or its extensions. History The superconducting properties of CeCu2Si2, a t ...
. Most notably, a LGR was used to reveal the linear temperature dependence of the magnetic penetration depth, characteristic of a d-wave superconductor, in a single crystal of YBa2Cu3O6.95. In these experiments, a superconducting sample is placed inside the bore of a LGR. The
diamagnetic Diamagnetic materials are repelled by a magnetic field; an applied magnetic field creates an induced magnetic field in them in the opposite direction, causing a repulsive force. In contrast, paramagnetic and ferromagnetic materials are attracted ...
response of the superconductor alters in the inductance of the LGR and, therefore, its resonant frequency. As described below, tracking the change in the resonant frequency as the temperature of the sample is changed allows one to deduce the temperature dependence of the magnetic penetration depth.


Theory

The inductance of the LGR can be expressed as L=\mu_0 V_\mathrm/\ell^2, where V_\mathrm is the volume of the LGR bore. Since the resonant frequency f_0 of the LGR is proportional to L^, a small change in the effective volume of the resonator bore will result in a change in the resonant frequency given by : \delta f_0 = -\frac \frac\,. Due to the
Meissner effect The Meissner effect (or Meissner–Ochsenfeld effect) is the expulsion of a magnetic field from a superconductor during its transition to the superconducting state when it is cooled below the critical temperature. This expulsion will repel a n ...
, when a superconducting sample is place in the bore of a LGR, the magnetic flux is expelled from the interior of the sample to within a penetration depth \lambda of its surface. Therefore, the effective volume of the resonator bore is reduced by an amount equal to the volume from which the magnetic flux has been excluded. This excluded volume is given by : V_\mathrm \approx ab\left(c-2\lambda_a\right)\,, where a, b, and c are the sample dimensions along the three
crystallographic Crystallography is the experimental science of determining the arrangement of atoms in crystalline solids. Crystallography is a fundamental subject in the fields of materials science and solid-state physics (condensed matter physics). The word ...
directions and abc is the sample volume V_\mathrm. In the above expression, it has been assumed that the microwave magnetic field is applied parallel to the b-axis of the sample. Since the presence of the superconductor reduces the LGR volume, \delta V_\mathrm=-V_\mathrm and : \delta f_0 = \frac \left(V_\mathrm-2ab\lambda_a\right)\,. Solving this expression for the a-axis penetration depth yields : \lambda_a = \frac-\frac\frac\,. Generally, it is not possible to use LGR frequency-shift measurements to determine the absolute value of the penetration depth because it would require knowing the sample thickness c very precisely. For example, in fully doped YBa2Cu3O7, \lambda_a\approx 100~\mathrm at low temperature. Therefore, to use the LGR measurement to determine \lambda_a to within 10%, one would have to know the value of c with an accuracy of 10~\mathrm which is typically not possible. Instead, the strategy is to track the changes in frequency as the sample temperature varies (while keeping the LGR at a fixed temperature). The absolute penetration depth can be expressed as : \lambda_a(T) = \lambda_a(T_0)+\Delta\lambda_a(T)\,, where T is temperature, T_0 is the experimental base temperature, and \Delta\lambda_a(T) is the change in penetration depth as the sample temperature is increased above the base temperature. One can, therefore, express the change in penetration depth as : \Delta\lambda_a(T) = \lambda_a(T)-\lambda_a(T_0)=-\frac\frac\left delta f_0(T)-\delta f_0(T_0)\right,. Finally, defining \Delta f_0(T)=\delta f_0(T)-\delta f_0(T_0), one has : \Delta\lambda_a(T) = -\frac\frac\,. This final expression shows how the LGR shifts in resonant frequency can be used to determine the temperature dependence of the magnetic penetration depth in a superconducting sample.


Experimental details

In a d-wave superconductor, the penetration depth typically changes by a few
ångström The angstromEntry "angstrom" in the Oxford online dictionary. Retrieved on 2019-03-02 from https://en.oxforddictionaries.com/definition/angstrom.Entry "angstrom" in the Merriam-Webster online dictionary. Retrieved on 2019-03-02 from https://www.m ...
s per degree
kelvin The kelvin, symbol K, is the primary unit of temperature in the International System of Units (SI), used alongside its prefixed forms and the degree Celsius. It is named after the Belfast-born and University of Glasgow-based engineer and phys ...
, which corresponds to \Delta f_0/f_0\sim 10^ for a 1~\mathrm^2 platelet sample in a LGR with a bore volume of 1~\mathrm^3. Measuring such small changes in relative frequency requires an extremely high-Q resonator. The ultrahigh quality factors are obtained by coating the LGR surfaces with a superconducting material, such as a lead-tin alloy. The resonator is then cooled below the superconducting transition temperature of the coating using a bath of
superfluid Superfluidity is the characteristic property of a fluid with zero viscosity which therefore flows without any loss of kinetic energy. When stirred, a superfluid forms vortices that continue to rotate indefinitely. Superfluidity occurs in two ...
liquid helium Liquid helium is a physical state of helium at very low temperatures at standard atmospheric pressures. Liquid helium may show superfluidity. At standard pressure, the chemical element helium exists in a liquid form only at the extremely low temp ...
. Quality factors of 10^6 have been achieved using copper LGRs coated with lead-tin and cooled to 1~\mathrm.


Measuring permittivity and permeability

This section describes how LGRs can be used to determine the electromagnetic properties of materials. When there are no materials filling either the gap or bore of the resonator, the impedance Z of the LGR can be expressed as : Z = R+j\omega L +\frac\,, where j=\sqrt. Re-expressed in terms of the resonant frequency \omega_0 and quality factor Q, the impedance is given by : \frac = \frac+j\left(\frac - \frac\right)\,. A measurement of the frequency dependence of the impedance of an empty LGR can be used to determine \omega_0 and Q. The impedance measurement is most easily done using the vector network analyzer (VNA) to measure the reflection coefficient S_ from an inductively-coupled LGR. The impedance and reflection coefficient are related by : S_ = \frac\,, where Z_0 is the output impedance of the VNA (usually, Z_0=50~\Omega)).


Complex permittivity

Now suppose that the gap of resonator has been completely filled with a dielectric material that has complex
relative permittivity The relative permittivity (in older texts, dielectric constant) is the permittivity of a material expressed as a ratio with the electric permittivity of a vacuum. A dielectric is an insulating material, and the dielectric constant of an insulat ...
\varepsilon_\mathrm=\varepsilon^\prime-j\varepsilon^. In this case, the effective capacitance becomes \varepsilon_\mathrmC and the impedance of the LGR is given by : Z_\varepsilon = R+j\omega L +\frac\,. Separating the real and imaginary terms leads to : Z_\varepsilon = \left +\left(\frac\right)\frac\right+j\left omega L-\left(\frac\right)\frac\right,. This expression shows that a nonzero \varepsilon^ enhances the effective resistance of the LGR and, therefore, lowers its quality factor. A nonzero \varepsilon^, on the other hand, alters the imaginary part of the impedance and modifies the resonant frequency. Written in terms of the empty-resonator resonant frequency and quality factor, the above impedance can be expressed as : \frac = \left frac+\left(\frac\right)\frac\right+j\left frac-\left(\frac\right)\frac\right,. Provided that \omega_0 and Q are known before hand, a measurement of the frequency dependence of Z_\varepsilon can be used to determine \varepsilon^\prime and \varepsilon^ of the material filling the gap of the LGR. This analysis gives the values of \varepsilon^\prime and \varepsilon^ at the resonant frequency of the filled LGR.


Complex permeability

Next, suppose that the bore of a LGR is filled with a magnetic material have complex
relative permeability In multiphase flow in porous media, the relative permeability of a phase is a dimensionless measure of the effective permeability of that phase. It is the ratio of the effective permeability of that phase to the absolute permeability. It can be v ...
\mu_\mathrm=\mu^\prime-j\mu^. In this case, the effective inductance becomes \mu_\mathrmL and the impedance of the LGR is given by : Z_\mu = R+j\omega \left(\mu^\prime-j\mu^\right) L +\frac\,. Separating Z_\mu into its real and imaginary components and writing the impedance in terms of \omega_0 and Q of the empty LGR yields : \frac = \left frac+\mu^\frac\rightj \left mu^\prime\frac-\frac\right,. Once again, \mu^ contributes additional dissipation which lowers the quality factor of the filled resonator and \mu^\prime shifts the resonant frequency. A measurement of the frequency dependence of Z_\mu can be used to extract the values of \mu^\prime and \mu^ at the resonant frequency of the filled LGR.


References

{{reflist Resonators