Evaporating Dish
   HOME

TheInfoList



OR:

An evaporating dish is a piece of
laboratory glassware Laboratory glassware refers to a variety of equipment used in scientific work, and traditionally made of glass. Glass can be blown, bent, cut, molded, and formed into many sizes and shapes, and is therefore common in chemistry, biology, and anal ...
used for the
evaporation Evaporation is a type of vaporization that occurs on the surface of a liquid as it changes into the gas phase. High concentration of the evaporating substance in the surrounding gas significantly slows down evaporation, such as when humidi ...
of solutions and
supernatant In an aqueous solution, precipitation is the process of transforming a dissolved substance into an insoluble solid from a super-saturated solution. The solid formed is called the precipitate. In case of an inorganic chemical reaction leading ...
liquids, and sometimes to their
melting point The melting point (or, rarely, liquefaction point) of a substance is the temperature at which it changes state from solid to liquid. At the melting point the solid and liquid phase exist in equilibrium. The melting point of a substance depends ...
. Evaporating dishes are used to evaporate excess solvents – most commonly water – to produce a concentrated solution or a solid precipitate of the dissolved substance. Most are made of
porcelain Porcelain () is a ceramic material made by heating substances, generally including materials such as kaolinite, in a kiln to temperatures between . The strength and translucence of porcelain, relative to other types of pottery, arises mainl ...
or
borosilicate glass Borosilicate glass is a type of glass with silica and boron trioxide as the main glass-forming constituents. Borosilicate glasses are known for having very low coefficients of thermal expansion (≈3 × 10−6 K−1 at 20 °C), ma ...
. Shallow glass evaporating dishes are commonly termed "watch glasses", since they resemble the front window of a
pocket watch A pocket watch (or pocketwatch) is a watch that is made to be carried in a pocket, as opposed to a watch, wristwatch, which is strapped to the wrist. They were the most common type of watch from their development in the 16th century until wr ...
. Some used for high-temperature work are of
refractory metal Refractory metals are a class of metals that are extraordinarily resistant to heat and wear. The expression is mostly used in the context of materials science, metallurgy and engineering. The definition of which elements belong to this group diff ...
s, usually of
platinum Platinum is a chemical element with the symbol Pt and atomic number 78. It is a dense, malleable, ductile, highly unreactive, precious, silverish-white transition metal. Its name originates from Spanish , a diminutive of "silver". Platinu ...
, owing to its non-reactive behaviour and low risk of contamination. The capacity of evaporators is usually small – in the range 3–10  ml. Larger dishes, up to 100 ml, are different in shape, and are more hemispherical. The evaporator is used most often in quantitative analysis. In the determination of
silicon Silicon is a chemical element with the symbol Si and atomic number 14. It is a hard, brittle crystalline solid with a blue-grey metallic luster, and is a tetravalent metalloid and semiconductor. It is a member of group 14 in the periodic tab ...
content in an organic sample, a small and accurately-measured quantity of a substance is added to the large amount of
sulfuric acid Sulfuric acid (American spelling and the preferred IUPAC name) or sulphuric acid ( Commonwealth spelling), known in antiquity as oil of vitriol, is a mineral acid composed of the elements sulfur, oxygen and hydrogen, with the molecular formu ...
, then heated in an evaporating dish. The dish is heated with a
Bunsen burner A Bunsen burner, named after Robert Bunsen, is a kind of ambient air gas burner used as laboratory equipment; it produces a single open gas flame, and is used for heating, sterilization, and combustion. The gas can be natural gas (which is main ...
, until only stable precipitate remains, which contains the silica content. The dish is then closed and heated at high temperature until completely clean, fused silica is produced. Comparison of the initial weight of the substance and that of the fused silica allows the content of silicon in the sample to be determined. The shape of the evaporating dish encourages evaporation in two ways: * The shell is relatively flat. A relatively large liquid surface promotes evaporation. * If heated in a flask or beaker, a part of the evaporated liquid condenses on the vessel walls and flows back into the solution. This does not happen in a dish. When heating liquid in an evaporating dish, the low walls encourage splashes and so stirring or swirling of evaporating liquids is considered bad practice, owing to the risk of spillage. Evaporation, especially in production quantities rather than merely for analysis, is now mostly performed in a
rotary evaporator A rotary evaporator (rotovap) is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. When referenced in the chemistry research literature, description of the use of this technique and ...
. This is preferred because it works much faster and may be used under vacuum, avoiding unwanted reactions with the atmosphere and allowing control of noxious fumes. Evaporation under vacuum also reduces the severity of bumping and violent ebullition.


See also

*
Crucible A crucible is a ceramic or metal container in which metals or other substances may be melted or subjected to very high temperatures. While crucibles were historically usually made from clay, they can be made from any material that withstands te ...


Notes


References

{{Laboratory equipment Laboratory glassware Laboratory porcelainware