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Borax Bead Test
The bead test is a traditional part of qualitative inorganic analysis to test for the presence of certain metals. The oldest one is the borax bead test or blister test. It was introduced by Berzelius in 1812.''Materials Handbook: A Concise Desktop Reference'', François Cardarell/ref> Since then other salts were used as fluxing agents, such as sodium carbonate or sodium fluoride. The most important one after borax is microcosmic salt, which is the basis of the microcosmic salt bead test. Borax bead A small loop is made in the end of a platinum wire and heated in a Bunsen burner flame until red hot. A stick made of another inert substance such as a magnesia stick (MgO) may also be used. It is then dipped into powdered borax and held in the hottest part of the flame where it swells up as it loses its water of crystallization and then shrinks, forming a colourless, transparent glass-like bead (a mixture of sodium metaborate and boric anhydride). The bead is allowed to cool and the ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |
Qualitative Inorganic Analysis
Classical qualitative inorganic analysis is a method of analytical chemistry which seeks to find the elemental composition of inorganic compounds. It is mainly focused on detecting ions in an aqueous solution, therefore materials in other forms may need to be brought to this state before using standard methods. The solution is then treated with various reagents to test for reactions characteristic of certain ions, which may cause color change, precipitation and other visible changes. Qualitative inorganic analysis is that branch or method of analytical chemistry which seeks to establish the elemental composition of inorganic compounds through various reagents. Physical appearance of inorganic salts Detecting cations According to their properties, cations are usually classified into six groups. Each group has a common reagent which can be used to separate them from the solution. To obtain meaningful results, the separation must be done in the sequence specified below, as some ... [...More Info...] [...Related Items...] OR: [Wikipedia] [Google] [Baidu] |